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The Heck reaction under ball-milling conditions

Tullberg, Erik LU ; Peters, D and Frejd, Torbjörn LU (2004) In Journal of Organometallic Chemistry 689(23). p.3778-3781
Abstract
The synthesis of unsaturated unnatural amino acids according to the Heck-Jeffery protocol using a ball-milling procedure is presented. NOE data recorded on the products confirm that the Z-isomer is formed. This type of mechano-chemistry provides an efficient, "solvent free" and reliable method for the synthesis of substituted dehydroalanines. These conditions provide patterns of reactivity complementary to conventional procedures. (C) 2004 Elsevier B.V. All rights reserved.
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author
organization
publishing date
type
Contribution to journal
publication status
published
subject
in
Journal of Organometallic Chemistry
volume
689
issue
23
pages
3778 - 3781
publisher
Elsevier
external identifiers
  • wos:000225312600013
  • scopus:19344361996
ISSN
0022-328X
DOI
10.1016/j.jorganchem.2004.06.045
language
English
LU publication?
yes
id
3fd15232-d396-4d08-9fa5-3a0243b4a2b6 (old id 139413)
date added to LUP
2007-07-10 14:52:54
date last changed
2017-12-10 04:33:36
@article{3fd15232-d396-4d08-9fa5-3a0243b4a2b6,
  abstract     = {The synthesis of unsaturated unnatural amino acids according to the Heck-Jeffery protocol using a ball-milling procedure is presented. NOE data recorded on the products confirm that the Z-isomer is formed. This type of mechano-chemistry provides an efficient, "solvent free" and reliable method for the synthesis of substituted dehydroalanines. These conditions provide patterns of reactivity complementary to conventional procedures. (C) 2004 Elsevier B.V. All rights reserved.},
  author       = {Tullberg, Erik and Peters, D and Frejd, Torbjörn},
  issn         = {0022-328X},
  language     = {eng},
  number       = {23},
  pages        = {3778--3781},
  publisher    = {Elsevier},
  series       = {Journal of Organometallic Chemistry},
  title        = {The Heck reaction under ball-milling conditions},
  url          = {http://dx.doi.org/10.1016/j.jorganchem.2004.06.045},
  volume       = {689},
  year         = {2004},
}