Characterization of polyacrylamide based monolithic columns
(2004) In Journal of Separation Science 27(10-11). p.828-836- Abstract
- Supermacroporous monolithic polyacrylamide (pAAm)-based columns have been prepared by radical cryo-copolymerization (copolymerization in the moderately frozen system) of acrylamide with functional co-monomer, allyl glycidyl ether (AGE), and cross-linker NN'-methylene-bis-acrylamide (MBAAm) directly in glass columns (ID 10 mm). The monolithic columns have uniform supermacroporous sponge-like structure with interconnected supermacropores of pore size 5-100 mum. The monoliths can be dried and stored in the dry state. High mechanical stability of the monoliths allowed sterilization by autoclaving. Column-to-column reproducibility of pAAm-monoliths was demonstrated on 5 monolithic columns from different batches prepared under the same... (More)
- Supermacroporous monolithic polyacrylamide (pAAm)-based columns have been prepared by radical cryo-copolymerization (copolymerization in the moderately frozen system) of acrylamide with functional co-monomer, allyl glycidyl ether (AGE), and cross-linker NN'-methylene-bis-acrylamide (MBAAm) directly in glass columns (ID 10 mm). The monolithic columns have uniform supermacroporous sponge-like structure with interconnected supermacropores of pore size 5-100 mum. The monoliths can be dried and stored in the dry state. High mechanical stability of the monoliths allowed sterilization by autoclaving. Column-to-column reproducibility of pAAm-monoliths was demonstrated on 5 monolithic columns from different batches prepared under the same cryostructuration conditions. (Less)
Please use this url to cite or link to this publication:
https://lup.lub.lu.se/record/140621
- author
- Plieva, Fatima LU ; Andersson, Jonatan LU ; Galaev, Igor LU and Mattiasson, Bo LU
- organization
- publishing date
- 2004
- type
- Contribution to journal
- publication status
- published
- subject
- in
- Journal of Separation Science
- volume
- 27
- issue
- 10-11
- pages
- 828 - 836
- publisher
- John Wiley & Sons Inc.
- external identifiers
-
- pmid:15354560
- wos:000222856300009
- scopus:4344717800
- ISSN
- 1615-9314
- DOI
- 10.1002/jssc.200401836
- language
- English
- LU publication?
- yes
- id
- c564d004-c25e-4521-bcdf-f8fba0c88640 (old id 140621)
- alternative location
- http://www.ncbi.nlm.nih.gov/sites/entrez?cmd=Retrieve&db=PubMed&list_uids=15354560&dopt=Abstract
- date added to LUP
- 2016-04-01 11:58:46
- date last changed
- 2022-04-13 04:15:35
@article{c564d004-c25e-4521-bcdf-f8fba0c88640,
abstract = {{Supermacroporous monolithic polyacrylamide (pAAm)-based columns have been prepared by radical cryo-copolymerization (copolymerization in the moderately frozen system) of acrylamide with functional co-monomer, allyl glycidyl ether (AGE), and cross-linker NN'-methylene-bis-acrylamide (MBAAm) directly in glass columns (ID 10 mm). The monolithic columns have uniform supermacroporous sponge-like structure with interconnected supermacropores of pore size 5-100 mum. The monoliths can be dried and stored in the dry state. High mechanical stability of the monoliths allowed sterilization by autoclaving. Column-to-column reproducibility of pAAm-monoliths was demonstrated on 5 monolithic columns from different batches prepared under the same cryostructuration conditions.}},
author = {{Plieva, Fatima and Andersson, Jonatan and Galaev, Igor and Mattiasson, Bo}},
issn = {{1615-9314}},
language = {{eng}},
number = {{10-11}},
pages = {{828--836}},
publisher = {{John Wiley & Sons Inc.}},
series = {{Journal of Separation Science}},
title = {{Characterization of polyacrylamide based monolithic columns}},
url = {{http://dx.doi.org/10.1002/jssc.200401836}},
doi = {{10.1002/jssc.200401836}},
volume = {{27}},
year = {{2004}},
}