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Systematic errors in isothermal micro- and nanocalorimetry

Wadsö, Ingemar LU and Wadsö, Lars LU (2005) In Journal of Thermal Analysis and Calorimetry 82(3). p.553-558
Abstract
Results of calorimetric measurements are easily impaired by different kinds of systematic errors. Isothermal micro- and nanocalorimeters are particularly sensitive to such errors, as the measured thermal powers are very low. In this paper the occurrence and effects of such errors are discussed: calibration errors, baseline errors, problems with evaporation/condensation, sorption, pV-work, gaseous reactants and different kinds of mechanical effects. Several numerical examples are given.
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author
organization
publishing date
type
Contribution to journal
publication status
published
subject
in
Journal of Thermal Analysis and Calorimetry
volume
82
issue
3
pages
553 - 558
publisher
Akademiai Kiado
external identifiers
  • wos:000234570800004
  • scopus:30444455469
ISSN
1588-2926
DOI
10.1007/s10973-005-0933-x
language
English
LU publication?
yes
id
0c091660-d7d7-4e99-bce7-b092ce5257f3 (old id 157659)
alternative location
http://springerlink.metapress.com/content/f2105m8512681283/?p=635c9466cb2f46ceac6c96ee09d905cc&pi=1
date added to LUP
2007-07-03 12:45:08
date last changed
2017-11-19 03:38:43
@article{0c091660-d7d7-4e99-bce7-b092ce5257f3,
  abstract     = {Results of calorimetric measurements are easily impaired by different kinds of systematic errors. Isothermal micro- and nanocalorimeters are particularly sensitive to such errors, as the measured thermal powers are very low. In this paper the occurrence and effects of such errors are discussed: calibration errors, baseline errors, problems with evaporation/condensation, sorption, pV-work, gaseous reactants and different kinds of mechanical effects. Several numerical examples are given.},
  author       = {Wadsö, Ingemar and Wadsö, Lars},
  issn         = {1588-2926},
  language     = {eng},
  number       = {3},
  pages        = {553--558},
  publisher    = {Akademiai Kiado},
  series       = {Journal of Thermal Analysis and Calorimetry},
  title        = {Systematic errors in isothermal micro- and nanocalorimetry},
  url          = {http://dx.doi.org/10.1007/s10973-005-0933-x},
  volume       = {82},
  year         = {2005},
}