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Solvent-free synthesis of chiral molecularly imprinted polymers: Porosity control using a nano-sized solid porogen

Duarte, Mariana LU ; Billing, Johan and Yilmaz, Ecevit (2016) In Journal of Applied Polymer Science 133(41). p.44104-44104
Abstract
Molecularly imprinted polymers (MIPs) have been synthesized in the absence of a solvent using fumed silica nanoparticles to create a porous network. The method employed led to a chiral imprinting effect and allowed for an excellent control over the internal morphology of imprinted and non-imprinted polymer (NIP) materials. The polymers possess high surface areas (>300 m2) and identical pore size (112 Å). The MIP exhibited an imprinting factor (IF) of 9 and a selectivity value (α) of 1.83 for (−)-ephedrine.
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author
; and
organization
publishing date
type
Contribution to journal
publication status
published
subject
in
Journal of Applied Polymer Science
volume
133
issue
41
pages
5 pages
publisher
John Wiley & Sons Inc.
external identifiers
  • scopus:84978926964
  • wos:000380728200027
ISSN
1097-4628
DOI
10.1002/app.44104
language
English
LU publication?
yes
id
26bafbd1-84e6-498d-b57e-2b817a10c8a5
date added to LUP
2016-09-21 11:45:31
date last changed
2022-02-21 20:34:42
@article{26bafbd1-84e6-498d-b57e-2b817a10c8a5,
  abstract     = {{Molecularly imprinted polymers (MIPs) have been synthesized in the absence of a solvent using fumed silica nanoparticles to create a porous network. The method employed led to a chiral imprinting effect and allowed for an excellent control over the internal morphology of imprinted and non-imprinted polymer (NIP) materials. The polymers possess high surface areas (>300 m2) and identical pore size (112 Å). The MIP exhibited an imprinting factor (IF) of 9 and a selectivity value (α) of 1.83 for (−)-ephedrine.}},
  author       = {{Duarte, Mariana and Billing, Johan and Yilmaz, Ecevit}},
  issn         = {{1097-4628}},
  language     = {{eng}},
  month        = {{07}},
  number       = {{41}},
  pages        = {{44104--44104}},
  publisher    = {{John Wiley & Sons Inc.}},
  series       = {{Journal of Applied Polymer Science}},
  title        = {{Solvent-free synthesis of chiral molecularly imprinted polymers: Porosity control using a nano-sized solid porogen}},
  url          = {{http://dx.doi.org/10.1002/app.44104}},
  doi          = {{10.1002/app.44104}},
  volume       = {{133}},
  year         = {{2016}},
}