Fast acquisition protocol for X-ray scattering tensor tomography
Kim, Jisoo ; Kagias, Matias LU
; Marone, Federica
; Shi, Zhitian
and Stampanoni, Marco
(2021)
In Scientific Reports
11(1).
p.23046-23046
- Abstract
Microstructural information over an entire sample is important to understand the macroscopic behaviour of materials. X-ray scattering tensor tomography facilitates the investigation of the microstructural organisation in statistically large sample volumes. However, established acquisition protocols based on scanning small-angle X-ray scattering and X-ray grating interferometry inherently require long scan times even with highly brilliant X-ray sources. Recent developments in X-ray diffractive optics towards circular pattern arrays enable fast single-shot acquisition of the sample scattering properties with 2D omnidirectional sensitivity. X-ray scattering tensor tomography with the use of this circular grating array has been... (More)
Microstructural information over an entire sample is important to understand the macroscopic behaviour of materials. X-ray scattering tensor tomography facilitates the investigation of the microstructural organisation in statistically large sample volumes. However, established acquisition protocols based on scanning small-angle X-ray scattering and X-ray grating interferometry inherently require long scan times even with highly brilliant X-ray sources. Recent developments in X-ray diffractive optics towards circular pattern arrays enable fast single-shot acquisition of the sample scattering properties with 2D omnidirectional sensitivity. X-ray scattering tensor tomography with the use of this circular grating array has been demonstrated. We propose here simple yet inherently rapid acquisition protocols for X-ray scattering tensor tomography leveraging on these new optical elements. Results from both simulation and experimental data, supported by a null space analysis, suggest that the proposed acquisition protocols are not only rapid but also corroborate that sufficient information for the accurate volumetric reconstruction of the scattering properties is provided. The proposed acquisition protocols will build the basis for rapid inspection and/or time-resolved tensor tomography of the microstructural organisation over an extended field of view.
(Less)
- author
- Kim, Jisoo
; Kagias, Matias
LU
; Marone, Federica
; Shi, Zhitian
and Stampanoni, Marco
- publishing date
- 2021-11-29
- type
- Contribution to journal
- publication status
- published
- subject
- in
- Scientific Reports
- volume
- 11
- issue
- 1
- pages
- 23046 - 23046
- publisher
- Nature Publishing Group
- external identifiers
-
- scopus:85120080044
- pmid:34845280
- ISSN
- 2045-2322
- DOI
- 10.1038/s41598-021-02467-w
- language
- English
- LU publication?
- no
- additional info
- © 2021. The Author(s).
- id
- 2d1f9706-a112-42ae-861e-45e4568491f6
- date added to LUP
- 2023-11-27 08:48:59
- date last changed
- 2024-06-21 14:23:19
@article{2d1f9706-a112-42ae-861e-45e4568491f6,
abstract = {{<p>Microstructural information over an entire sample is important to understand the macroscopic behaviour of materials. X-ray scattering tensor tomography facilitates the investigation of the microstructural organisation in statistically large sample volumes. However, established acquisition protocols based on scanning small-angle X-ray scattering and X-ray grating interferometry inherently require long scan times even with highly brilliant X-ray sources. Recent developments in X-ray diffractive optics towards circular pattern arrays enable fast single-shot acquisition of the sample scattering properties with 2D omnidirectional sensitivity. X-ray scattering tensor tomography with the use of this circular grating array has been demonstrated. We propose here simple yet inherently rapid acquisition protocols for X-ray scattering tensor tomography leveraging on these new optical elements. Results from both simulation and experimental data, supported by a null space analysis, suggest that the proposed acquisition protocols are not only rapid but also corroborate that sufficient information for the accurate volumetric reconstruction of the scattering properties is provided. The proposed acquisition protocols will build the basis for rapid inspection and/or time-resolved tensor tomography of the microstructural organisation over an extended field of view.</p>}},
author = {{Kim, Jisoo and Kagias, Matias and Marone, Federica and Shi, Zhitian and Stampanoni, Marco}},
issn = {{2045-2322}},
language = {{eng}},
month = {{11}},
number = {{1}},
pages = {{23046--23046}},
publisher = {{Nature Publishing Group}},
series = {{Scientific Reports}},
title = {{Fast acquisition protocol for X-ray scattering tensor tomography}},
url = {{http://dx.doi.org/10.1038/s41598-021-02467-w}},
doi = {{10.1038/s41598-021-02467-w}},
volume = {{11}},
year = {{2021}},
}