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The use of in situ and ex situ techniques for the study of the formation mechanism of mesoporous silica formed with non-ionic triblock copolymers.

Kjellman, Tomas LU and Alfredsson, Viveka LU (2013) In Chemical Society Reviews 42(9). p.3777-3791
Abstract
Since the discovery of the mesoporous silica material templated by ionic surfactants and the subsequent development of materials templated by non-ionic surfactants and polymers, for example SBA-15, there has been a continuous research effort towards understanding their formation. In situ methodologies, such as Small Angle X-ray Scattering (SAXS), Small Angle Neutron Scattering (SANS), spectroscopic techniques like NMR and EPR, and ex situ methodologies such as electron microscopy techniques (SEM, TEM and cryo-TEM) are powerful and important tools in the investigation of the mechanism by which these materials form. The need for a fundamental understanding of the systems is of academic concern and of great importance when developing... (More)
Since the discovery of the mesoporous silica material templated by ionic surfactants and the subsequent development of materials templated by non-ionic surfactants and polymers, for example SBA-15, there has been a continuous research effort towards understanding their formation. In situ methodologies, such as Small Angle X-ray Scattering (SAXS), Small Angle Neutron Scattering (SANS), spectroscopic techniques like NMR and EPR, and ex situ methodologies such as electron microscopy techniques (SEM, TEM and cryo-TEM) are powerful and important tools in the investigation of the mechanism by which these materials form. The need for a fundamental understanding of the systems is of academic concern and of great importance when developing materials for applications. In this tutorial review we aim to give the reader a comprehensive overview on the development of the field over the years and an introduction to the experimental in situ and ex situ techniques that have been used. (Less)
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author
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organization
publishing date
type
Contribution to journal
publication status
published
subject
in
Chemical Society Reviews
volume
42
issue
9
pages
3777 - 3791
publisher
Royal Society of Chemistry
external identifiers
  • wos:000317596100010
  • pmid:23093089
  • scopus:84884608327
ISSN
0306-0012
DOI
10.1039/c2cs35298b
language
English
LU publication?
yes
id
3e091a85-9d3a-4238-8200-e2a3d5871aa4 (old id 3160440)
alternative location
http://www.ncbi.nlm.nih.gov/pubmed/23093089?dopt=Abstract
date added to LUP
2016-04-01 11:15:51
date last changed
2023-11-10 15:47:38
@article{3e091a85-9d3a-4238-8200-e2a3d5871aa4,
  abstract     = {{Since the discovery of the mesoporous silica material templated by ionic surfactants and the subsequent development of materials templated by non-ionic surfactants and polymers, for example SBA-15, there has been a continuous research effort towards understanding their formation. In situ methodologies, such as Small Angle X-ray Scattering (SAXS), Small Angle Neutron Scattering (SANS), spectroscopic techniques like NMR and EPR, and ex situ methodologies such as electron microscopy techniques (SEM, TEM and cryo-TEM) are powerful and important tools in the investigation of the mechanism by which these materials form. The need for a fundamental understanding of the systems is of academic concern and of great importance when developing materials for applications. In this tutorial review we aim to give the reader a comprehensive overview on the development of the field over the years and an introduction to the experimental in situ and ex situ techniques that have been used.}},
  author       = {{Kjellman, Tomas and Alfredsson, Viveka}},
  issn         = {{0306-0012}},
  language     = {{eng}},
  number       = {{9}},
  pages        = {{3777--3791}},
  publisher    = {{Royal Society of Chemistry}},
  series       = {{Chemical Society Reviews}},
  title        = {{The use of in situ and ex situ techniques for the study of the formation mechanism of mesoporous silica formed with non-ionic triblock copolymers.}},
  url          = {{http://dx.doi.org/10.1039/c2cs35298b}},
  doi          = {{10.1039/c2cs35298b}},
  volume       = {{42}},
  year         = {{2013}},
}