The Heck reaction under ball-milling conditions
(2004) In Journal of Organometallic Chemistry 689(23). p.3778-3781- Abstract
- The synthesis of unsaturated unnatural amino acids according to the Heck-Jeffery protocol using a ball-milling procedure is presented. NOE data recorded on the products confirm that the Z-isomer is formed. This type of mechano-chemistry provides an efficient, "solvent free" and reliable method for the synthesis of substituted dehydroalanines. These conditions provide patterns of reactivity complementary to conventional procedures. (C) 2004 Elsevier B.V. All rights reserved.
Please use this url to cite or link to this publication:
https://lup.lub.lu.se/record/139413
- author
- Tullberg, Erik LU ; Peters, D and Frejd, Torbjörn LU
- organization
- publishing date
- 2004
- type
- Contribution to journal
- publication status
- published
- subject
- in
- Journal of Organometallic Chemistry
- volume
- 689
- issue
- 23
- pages
- 3778 - 3781
- publisher
- Elsevier
- external identifiers
-
- wos:000225312600013
- scopus:19344361996
- ISSN
- 0022-328X
- DOI
- 10.1016/j.jorganchem.2004.06.045
- language
- English
- LU publication?
- yes
- additional info
- The information about affiliations in this record was updated in December 2015. The record was previously connected to the following departments: Organic chemistry (S/LTH) (011001240)
- id
- 3fd15232-d396-4d08-9fa5-3a0243b4a2b6 (old id 139413)
- date added to LUP
- 2016-04-01 16:27:34
- date last changed
- 2022-03-22 18:48:24
@article{3fd15232-d396-4d08-9fa5-3a0243b4a2b6, abstract = {{The synthesis of unsaturated unnatural amino acids according to the Heck-Jeffery protocol using a ball-milling procedure is presented. NOE data recorded on the products confirm that the Z-isomer is formed. This type of mechano-chemistry provides an efficient, "solvent free" and reliable method for the synthesis of substituted dehydroalanines. These conditions provide patterns of reactivity complementary to conventional procedures. (C) 2004 Elsevier B.V. All rights reserved.}}, author = {{Tullberg, Erik and Peters, D and Frejd, Torbjörn}}, issn = {{0022-328X}}, language = {{eng}}, number = {{23}}, pages = {{3778--3781}}, publisher = {{Elsevier}}, series = {{Journal of Organometallic Chemistry}}, title = {{The Heck reaction under ball-milling conditions}}, url = {{http://dx.doi.org/10.1016/j.jorganchem.2004.06.045}}, doi = {{10.1016/j.jorganchem.2004.06.045}}, volume = {{689}}, year = {{2004}}, }