Advanced

In situ hydrogen loading on zirconium powder

Maimaitiyili, Tuerdi LU ; Blomqvist, Jakob; Steuwer, Axel LU ; Bjerkén, Christina LU ; Zanellato, Olivier; Blackmur, Matthew S.; Andrieux, Jerome and Ribeiro, Fabienne (2015) In Journal of Synchrotron Radiation 22. p.995-1000
Abstract
For the first time, various hydride phases in a zirconium-hydrogen system have been prepared in a high-energy synchrotron X-ray radiation beamline and their transformation behaviour has been studied in situ. First, the formation and dissolution of hydrides in commercially pure zirconium powder were monitored in real time during hydrogenation and dehydrogenation, then whole pattern crystal structure analysis such as Rietveld and Pawley refinements were performed. All commonly reported low-pressure phases presented in the Zr-H phase diagram are obtained from a single experimental arrangement.
Please use this url to cite or link to this publication:
author
organization
publishing date
type
Contribution to journal
publication status
published
subject
keywords
zirconium hydride, synchrotron X-ray diffraction, in situ hydrogen, charging, hydrogen-induced degradation, phase transformation
in
Journal of Synchrotron Radiation
volume
22
pages
995 - 1000
publisher
Wiley-Blackwell
external identifiers
  • wos:000357407900015
  • pmid:26134803
  • scopus:84937400779
ISSN
1600-5775
DOI
10.1107/S1600577515009054
language
English
LU publication?
yes
id
54233d73-56e0-4840-a22a-5fac44394025 (old id 7790862)
date added to LUP
2015-09-03 09:37:57
date last changed
2017-03-12 03:49:37
@article{54233d73-56e0-4840-a22a-5fac44394025,
  abstract     = {For the first time, various hydride phases in a zirconium-hydrogen system have been prepared in a high-energy synchrotron X-ray radiation beamline and their transformation behaviour has been studied in situ. First, the formation and dissolution of hydrides in commercially pure zirconium powder were monitored in real time during hydrogenation and dehydrogenation, then whole pattern crystal structure analysis such as Rietveld and Pawley refinements were performed. All commonly reported low-pressure phases presented in the Zr-H phase diagram are obtained from a single experimental arrangement.},
  author       = {Maimaitiyili, Tuerdi and Blomqvist, Jakob and Steuwer, Axel and Bjerkén, Christina and Zanellato, Olivier and Blackmur, Matthew S. and Andrieux, Jerome and Ribeiro, Fabienne},
  issn         = {1600-5775},
  keyword      = {zirconium hydride,synchrotron X-ray diffraction,in situ hydrogen,charging,hydrogen-induced degradation,phase transformation},
  language     = {eng},
  pages        = {995--1000},
  publisher    = {Wiley-Blackwell},
  series       = {Journal of Synchrotron Radiation},
  title        = {In situ hydrogen loading on zirconium powder},
  url          = {http://dx.doi.org/10.1107/S1600577515009054},
  volume       = {22},
  year         = {2015},
}