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Simultaneous Reciprocal and Real Space X-Ray Imaging of Time-Evolving Systems

Kagias, Matias LU ; Wang, Zhentian ; Lovric, Goran ; Jefimovs, Konstantins and Stampanoni, Marco (2021) In Physical Review Applied 15(4).
Abstract

Imaging the (sub)micron scale over large areas with high temporal resolution becomes increasingly necessary for the development and investigation of novel materials under realistic operation conditions. Small angle x-ray scattering imaging methods provide micro- and nanoscale structural information of materials. A fundamental shortcoming of such methods is the long acquisition time required to investigate macroscopic objects. In this work, we propose a single shot imaging method that allows reciprocal space sensitivity at a local level while maintaining spatial resolution for imaging macroscopic objects. We use an instrument that is sensitive to the ultrasmall angle x-ray scattering range and utilize it to image unstable polydisperse... (More)

Imaging the (sub)micron scale over large areas with high temporal resolution becomes increasingly necessary for the development and investigation of novel materials under realistic operation conditions. Small angle x-ray scattering imaging methods provide micro- and nanoscale structural information of materials. A fundamental shortcoming of such methods is the long acquisition time required to investigate macroscopic objects. In this work, we propose a single shot imaging method that allows reciprocal space sensitivity at a local level while maintaining spatial resolution for imaging macroscopic objects. We use an instrument that is sensitive to the ultrasmall angle x-ray scattering range and utilize it to image unstable polydisperse particle systems. This allows us to observe in real time the evolution of the local average particle diameter due to the stratification of the microparticles.

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Please use this url to cite or link to this publication:
author
; ; ; and
publishing date
type
Contribution to journal
publication status
published
subject
in
Physical Review Applied
volume
15
issue
4
article number
044038
publisher
American Physical Society
external identifiers
  • scopus:85105406879
ISSN
2331-7019
DOI
10.1103/PhysRevApplied.15.044038
language
English
LU publication?
no
additional info
Publisher Copyright: © 2021 American Physical Society.
id
7d8cece9-85bc-454a-a7d1-f075dc246b5a
date added to LUP
2023-11-27 08:58:43
date last changed
2023-12-04 11:54:02
@article{7d8cece9-85bc-454a-a7d1-f075dc246b5a,
  abstract     = {{<p>Imaging the (sub)micron scale over large areas with high temporal resolution becomes increasingly necessary for the development and investigation of novel materials under realistic operation conditions. Small angle x-ray scattering imaging methods provide micro- and nanoscale structural information of materials. A fundamental shortcoming of such methods is the long acquisition time required to investigate macroscopic objects. In this work, we propose a single shot imaging method that allows reciprocal space sensitivity at a local level while maintaining spatial resolution for imaging macroscopic objects. We use an instrument that is sensitive to the ultrasmall angle x-ray scattering range and utilize it to image unstable polydisperse particle systems. This allows us to observe in real time the evolution of the local average particle diameter due to the stratification of the microparticles.</p>}},
  author       = {{Kagias, Matias and Wang, Zhentian and Lovric, Goran and Jefimovs, Konstantins and Stampanoni, Marco}},
  issn         = {{2331-7019}},
  language     = {{eng}},
  number       = {{4}},
  publisher    = {{American Physical Society}},
  series       = {{Physical Review Applied}},
  title        = {{Simultaneous Reciprocal and Real Space X-Ray Imaging of Time-Evolving Systems}},
  url          = {{http://dx.doi.org/10.1103/PhysRevApplied.15.044038}},
  doi          = {{10.1103/PhysRevApplied.15.044038}},
  volume       = {{15}},
  year         = {{2021}},
}