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Microwave Synthesis of Alkali-Free Hexaniobate, Decaniobate, and Hexatantalate Polyoxometalate Ions

Rambaran, Mark A. LU ; Pascual-Borràs, Magda and Ohlin, C. André (2019) In European Journal of Inorganic Chemistry 2019(35). p.3913-3918
Abstract

Microwave preparation of polyoxoniobates and -tantalates afford a more rapid alternative to conventional hydrothermal methods of synthesis, in addition to allowing for the use of anhydrous niobium pentoxide in lieu of niobic acid, albeit with diminished yields. Limitations associated with the pH at which different oxides can be activated and how this affects the accessibility of different products are also discussed.

Please use this url to cite or link to this publication:
author
; and
publishing date
type
Contribution to journal
publication status
published
keywords
Microwave synthesis, Niobium, Polyoxometalates, Synthesis design, Tantalum
in
European Journal of Inorganic Chemistry
volume
2019
issue
35
pages
6 pages
publisher
John Wiley & Sons Inc.
external identifiers
  • scopus:85072211990
ISSN
1434-1948
DOI
10.1002/ejic.201900750
language
English
LU publication?
no
additional info
Publisher Copyright: © 2019 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
id
90ed1ccc-ffb3-4aa3-b0b6-990938db2e04
date added to LUP
2023-02-15 16:54:43
date last changed
2025-01-11 21:40:20
@article{90ed1ccc-ffb3-4aa3-b0b6-990938db2e04,
  abstract     = {{<p>Microwave preparation of polyoxoniobates and -tantalates afford a more rapid alternative to conventional hydrothermal methods of synthesis, in addition to allowing for the use of anhydrous niobium pentoxide in lieu of niobic acid, albeit with diminished yields. Limitations associated with the pH at which different oxides can be activated and how this affects the accessibility of different products are also discussed.</p>}},
  author       = {{Rambaran, Mark A. and Pascual-Borràs, Magda and Ohlin, C. André}},
  issn         = {{1434-1948}},
  keywords     = {{Microwave synthesis; Niobium; Polyoxometalates; Synthesis design; Tantalum}},
  language     = {{eng}},
  month        = {{09}},
  number       = {{35}},
  pages        = {{3913--3918}},
  publisher    = {{John Wiley & Sons Inc.}},
  series       = {{European Journal of Inorganic Chemistry}},
  title        = {{Microwave Synthesis of Alkali-Free Hexaniobate, Decaniobate, and Hexatantalate Polyoxometalate Ions}},
  url          = {{http://dx.doi.org/10.1002/ejic.201900750}},
  doi          = {{10.1002/ejic.201900750}},
  volume       = {{2019}},
  year         = {{2019}},
}