Design of a humidity controlled sample stage for simultaneous conductivity and synchrotron X-ray scattering measurements.
(2013) In Review of Scientific Instruments 84(7).- Abstract
- We report on the design and operation of a novel sample stage, used to simultaneously measure X-ray scattering profiles and conductivity of a polymer electrolyte membrane (PEM) surrounded by humid air as a function of temperature and relative humidity. We present data obtained at the Advanced Light Source and Stanford Synchrotron Radiation Laboratory. We demonstrate precise humidity control and accurate determination of morphology and conductivity over a wide range of temperatures. The sample stage is used to study structure-property relationships of a semi-crystalline block copolymer PEM, sulfonated polystyrene-block-polyethylene.
Please use this url to cite or link to this publication:
https://lup.lub.lu.se/record/4006367
- author
- Jackson, Andrew LU ; Beers, Keith M ; Chen, X Chelsea ; Hexemer, Alexander ; Pople, John A ; Kerr, John B and Balsara, Nitash P
- organization
- publishing date
- 2013
- type
- Contribution to journal
- publication status
- published
- subject
- in
- Review of Scientific Instruments
- volume
- 84
- issue
- 7
- article number
- 075114
- publisher
- American Institute of Physics (AIP)
- external identifiers
-
- wos:000322602200077
- pmid:23902113
- scopus:84886737066
- pmid:23902113
- ISSN
- 1089-7623
- DOI
- 10.1063/1.4815981
- language
- English
- LU publication?
- yes
- id
- 99c981ae-4202-45d6-88b8-a0715aa9606e (old id 4006367)
- date added to LUP
- 2016-04-01 10:58:33
- date last changed
- 2022-02-25 07:25:40
@article{99c981ae-4202-45d6-88b8-a0715aa9606e, abstract = {{We report on the design and operation of a novel sample stage, used to simultaneously measure X-ray scattering profiles and conductivity of a polymer electrolyte membrane (PEM) surrounded by humid air as a function of temperature and relative humidity. We present data obtained at the Advanced Light Source and Stanford Synchrotron Radiation Laboratory. We demonstrate precise humidity control and accurate determination of morphology and conductivity over a wide range of temperatures. The sample stage is used to study structure-property relationships of a semi-crystalline block copolymer PEM, sulfonated polystyrene-block-polyethylene.}}, author = {{Jackson, Andrew and Beers, Keith M and Chen, X Chelsea and Hexemer, Alexander and Pople, John A and Kerr, John B and Balsara, Nitash P}}, issn = {{1089-7623}}, language = {{eng}}, number = {{7}}, publisher = {{American Institute of Physics (AIP)}}, series = {{Review of Scientific Instruments}}, title = {{Design of a humidity controlled sample stage for simultaneous conductivity and synchrotron X-ray scattering measurements.}}, url = {{http://dx.doi.org/10.1063/1.4815981}}, doi = {{10.1063/1.4815981}}, volume = {{84}}, year = {{2013}}, }