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Crystal structure of (piperidine-1-carbo-di-thio-ato-κ(2) S,S)[2-(pyridin-2-yl)phenyl-κ(2) C (1),N]palladium(II).

Kondrashov, Mikhail LU ; Fleckhaus, André LU ; Gritcenko, Roman and Wendt, Ola LU (2015) In Acta crystallographica. Section E: Crystallographic communications 71(Pt 9). p.166-166
Abstract
The title compound, [Pd(C11H8N)(C6H10NS2)], crystallizes with three similar and discrete mol-ecules in the asymmetric unit. The CNS2 donor set defines a distorted square-planar geometry around the Pd(II) atom, with very small deviations from planarity. The bidentate nature of the ligands gives fairly large deviations from the ideal 90° angles; the C-Pd-N angles are all around 81° and the S-Pd-S angles are around 75°. Mol-ecules pack via dispersion inter-actions.
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author
; ; and
organization
publishing date
type
Contribution to journal
publication status
published
subject
in
Acta crystallographica. Section E: Crystallographic communications
volume
71
issue
Pt 9
pages
166 - 166
publisher
International Union of Crystallography
external identifiers
  • pmid:26396868
  • scopus:84953870386
  • wos:000370079100007
  • pmid:26396868
ISSN
2056-9890
DOI
10.1107/S2056989015015005
language
English
LU publication?
yes
id
9ae8a29a-dbd4-49ff-afca-b9169086938e (old id 8035172)
date added to LUP
2016-04-04 09:08:44
date last changed
2025-10-14 09:06:40
@article{9ae8a29a-dbd4-49ff-afca-b9169086938e,
  abstract     = {{The title compound, [Pd(C11H8N)(C6H10NS2)], crystallizes with three similar and discrete mol-ecules in the asymmetric unit. The CNS2 donor set defines a distorted square-planar geometry around the Pd(II) atom, with very small deviations from planarity. The bidentate nature of the ligands gives fairly large deviations from the ideal 90° angles; the C-Pd-N angles are all around 81° and the S-Pd-S angles are around 75°. Mol-ecules pack via dispersion inter-actions.}},
  author       = {{Kondrashov, Mikhail and Fleckhaus, André and Gritcenko, Roman and Wendt, Ola}},
  issn         = {{2056-9890}},
  language     = {{eng}},
  number       = {{Pt 9}},
  pages        = {{166--166}},
  publisher    = {{International Union of Crystallography}},
  series       = {{Acta crystallographica. Section E: Crystallographic communications}},
  title        = {{Crystal structure of (piperidine-1-carbo-di-thio-ato-κ(2) S,S)[2-(pyridin-2-yl)phenyl-κ(2) C (1),N]palladium(II).}},
  url          = {{http://dx.doi.org/10.1107/S2056989015015005}},
  doi          = {{10.1107/S2056989015015005}},
  volume       = {{71}},
  year         = {{2015}},
}