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Small-angle neutron scattering studies on the mesoporous molecular sieve MCM-41

Edler, Karen J. LU orcid ; Reynolds, Philip A. and White, John W. (1998) In Journal of Physical Chemistry B 102(19). p.3676-3683
Abstract

A pure silica MCM-41 preparation with high crystalline order perpendicular to the channels has been examined using small-angle neutron scattering and the contrast variation method in both the calcined and template-containing forms. This defines various structural features such as template and water distributions and content, local silica density, and surface properties. Adsorption isotherm data, NMR, previous neutron scattering data, and the SANS data allow a choice between proposed models for the channel structure of MCM-41, in terms of the straightness of the channels and their surface roughness.

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author
; and
publishing date
type
Contribution to journal
publication status
published
in
Journal of Physical Chemistry B
volume
102
issue
19
pages
8 pages
publisher
The American Chemical Society (ACS)
external identifiers
  • scopus:0001342292
ISSN
1520-6106
DOI
10.1021/jp971694
language
English
LU publication?
no
id
9fad606b-30b2-48de-9562-cdafaa5ada21
date added to LUP
2023-05-04 18:17:11
date last changed
2024-01-08 13:58:34
@article{9fad606b-30b2-48de-9562-cdafaa5ada21,
  abstract     = {{<p>A pure silica MCM-41 preparation with high crystalline order perpendicular to the channels has been examined using small-angle neutron scattering and the contrast variation method in both the calcined and template-containing forms. This defines various structural features such as template and water distributions and content, local silica density, and surface properties. Adsorption isotherm data, NMR, previous neutron scattering data, and the SANS data allow a choice between proposed models for the channel structure of MCM-41, in terms of the straightness of the channels and their surface roughness.</p>}},
  author       = {{Edler, Karen J. and Reynolds, Philip A. and White, John W.}},
  issn         = {{1520-6106}},
  language     = {{eng}},
  month        = {{05}},
  number       = {{19}},
  pages        = {{3676--3683}},
  publisher    = {{The American Chemical Society (ACS)}},
  series       = {{Journal of Physical Chemistry B}},
  title        = {{Small-angle neutron scattering studies on the mesoporous molecular sieve MCM-41}},
  url          = {{http://dx.doi.org/10.1021/jp971694}},
  doi          = {{10.1021/jp971694}},
  volume       = {{102}},
  year         = {{1998}},
}