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Chemically inert microfluidic flow regulator with a glass-Teflon2-glass structure fabricated via facile thermal bonding

Shen, Kao Mai ; Morikawa, Kyojiro ; Kitamori, Takehiko LU and Chen, Chihchen (2025) In Sensors and Actuators A: Physical 396.
Abstract

Recent advancements in integrated chemical microsystems have significantly enhanced the efficiency and precision of chemical synthesis. However, limitations in current materials and fabrication technologies pose challenges to developing robust flow regulation essential for system operation and scalability. This study presents a cleanroom-free, surface-modification-free bonding method for fabricating chemically inert microfluidic flow regulators with a glass-Teflon-glass structure. The fabrication process leverages the distinct melting temperatures of commercially available fluorinated ethylene propylene (FEP) and polytetrafluoroethylene (PTFE) films, utilizing their melting point differences to assign FEP as a thermal adhesive layer and... (More)

Recent advancements in integrated chemical microsystems have significantly enhanced the efficiency and precision of chemical synthesis. However, limitations in current materials and fabrication technologies pose challenges to developing robust flow regulation essential for system operation and scalability. This study presents a cleanroom-free, surface-modification-free bonding method for fabricating chemically inert microfluidic flow regulators with a glass-Teflon-glass structure. The fabrication process leverages the distinct melting temperatures of commercially available fluorinated ethylene propylene (FEP) and polytetrafluoroethylene (PTFE) films, utilizing their melting point differences to assign FEP as a thermal adhesive layer and PTFE as a movable diaphragm. The resulting flow regulator employs pneumatic pressure to control the system’s flow rate with linear and hysteresis-free performance. It withstands applied pressures up to 700 kPa—more than an order of magnitude higher than previously reported glass-Teflon valves—and operating temperatures as high as 150°C. Furthermore, the study demonstrates uniform flow distribution within a parallel microfluidic system designed for scalability and successful integration of multiple regulators into microfluidic channels. This practical and cost-effective fabrication method broadens the potential applications of chemically resistant microfluidic devices, particularly in chemical processes that require precise and reliable fluid control.

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author
; ; and
organization
publishing date
type
Contribution to journal
publication status
published
subject
keywords
Chemical resistance, Cleanroom-free bonding, Flow regulator, Glass-Teflon bonding, Microfluidic, Microvalve
in
Sensors and Actuators A: Physical
volume
396
article number
117220
publisher
Elsevier
external identifiers
  • scopus:105027200008
ISSN
0924-4247
DOI
10.1016/j.sna.2025.117220
language
English
LU publication?
yes
additional info
Publisher Copyright: © 2025 The Author(s). Published by Elsevier B.V. This is an open access article under the CC BY-NC-ND license. http://creativecommons.org/licenses/by-nc-nd/4.0/
id
b030b46a-a4c3-4f61-bcce-73b7df466bbb
date added to LUP
2026-02-11 13:27:30
date last changed
2026-02-11 13:28:31
@article{b030b46a-a4c3-4f61-bcce-73b7df466bbb,
  abstract     = {{<p>Recent advancements in integrated chemical microsystems have significantly enhanced the efficiency and precision of chemical synthesis. However, limitations in current materials and fabrication technologies pose challenges to developing robust flow regulation essential for system operation and scalability. This study presents a cleanroom-free, surface-modification-free bonding method for fabricating chemically inert microfluidic flow regulators with a glass-Teflon-glass structure. The fabrication process leverages the distinct melting temperatures of commercially available fluorinated ethylene propylene (FEP) and polytetrafluoroethylene (PTFE) films, utilizing their melting point differences to assign FEP as a thermal adhesive layer and PTFE as a movable diaphragm. The resulting flow regulator employs pneumatic pressure to control the system’s flow rate with linear and hysteresis-free performance. It withstands applied pressures up to 700 kPa—more than an order of magnitude higher than previously reported glass-Teflon valves—and operating temperatures as high as 150°C. Furthermore, the study demonstrates uniform flow distribution within a parallel microfluidic system designed for scalability and successful integration of multiple regulators into microfluidic channels. This practical and cost-effective fabrication method broadens the potential applications of chemically resistant microfluidic devices, particularly in chemical processes that require precise and reliable fluid control.</p>}},
  author       = {{Shen, Kao Mai and Morikawa, Kyojiro and Kitamori, Takehiko and Chen, Chihchen}},
  issn         = {{0924-4247}},
  keywords     = {{Chemical resistance; Cleanroom-free bonding; Flow regulator; Glass-Teflon bonding; Microfluidic; Microvalve}},
  language     = {{eng}},
  month        = {{12}},
  publisher    = {{Elsevier}},
  series       = {{Sensors and Actuators A: Physical}},
  title        = {{Chemically inert microfluidic flow regulator with a glass-Teflon<sup>2</sup>-glass structure fabricated via facile thermal bonding}},
  url          = {{http://dx.doi.org/10.1016/j.sna.2025.117220}},
  doi          = {{10.1016/j.sna.2025.117220}},
  volume       = {{396}},
  year         = {{2025}},
}