Rapid extraction of short-lived isotopes from a buffer gas cell for use in gas-phase chemistry experiments, Part II : On-line studies with short-lived accelerator-produced radionuclides
(2021) In Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms 507. p.27-35- Abstract
A novel combination of advanced gas-chromatography and detection systems coupled to a buffer-gas cell was characterized on-line to allow gas-phase chemical studies of accelerator-produced short-lived α-decaying mercury, francium, and astatine isotopes. These were produced in 40Ar- and 48Ca-induced nuclear fusion–evaporation reactions, subsequently isolated in the recoil separators MARS at Texas A&M University, USA, and TASCA at GSI Darmstadt, Germany, before being thermalized in a buffer-gas-stopping cell. From the latter, the nuclear reaction products were extracted into gas-phase chromatographic systems, suitable for registering α-decaying short-lived radionuclides, such as isotopes of superheavy elements.... (More)
A novel combination of advanced gas-chromatography and detection systems coupled to a buffer-gas cell was characterized on-line to allow gas-phase chemical studies of accelerator-produced short-lived α-decaying mercury, francium, and astatine isotopes. These were produced in 40Ar- and 48Ca-induced nuclear fusion–evaporation reactions, subsequently isolated in the recoil separators MARS at Texas A&M University, USA, and TASCA at GSI Darmstadt, Germany, before being thermalized in a buffer-gas-stopping cell. From the latter, the nuclear reaction products were extracted into gas-phase chromatographic systems, suitable for registering α-decaying short-lived radionuclides, such as isotopes of superheavy elements. Efficiencies of 21(3)% for 204-209Fr were reached for the extraction into the optimized miniCOMPACT gas-chromatography setup, indicating that this technique enables the identification of isotopes of volatile as well as non-volatile elements. These studies guide the path towards chemical investigations of superheavy elements beyond flerovium, which are out of reach with currently used setups.
(Less)
- author
- organization
- publishing date
- 2021-11-15
- type
- Contribution to journal
- publication status
- published
- subject
- keywords
- Buffer gas cell, Extraction efficiency, Extraction time, Fusion–evaporation reactions, Gas catcher, Heavy elements, Superheavy elements
- in
- Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms
- volume
- 507
- pages
- 9 pages
- publisher
- Elsevier
- external identifiers
-
- scopus:85115937383
- ISSN
- 0168-583X
- DOI
- 10.1016/j.nimb.2021.09.004
- language
- English
- LU publication?
- yes
- additional info
- Publisher Copyright: © 2021 Elsevier B.V.
- id
- b0ecea35-f117-4980-9cc9-bd81da49d9e8
- date added to LUP
- 2021-10-13 11:41:26
- date last changed
- 2022-04-27 04:43:11
@article{b0ecea35-f117-4980-9cc9-bd81da49d9e8, abstract = {{<p>A novel combination of advanced gas-chromatography and detection systems coupled to a buffer-gas cell was characterized on-line to allow gas-phase chemical studies of accelerator-produced short-lived α-decaying mercury, francium, and astatine isotopes. These were produced in <sup>40</sup>Ar- and <sup>48</sup>Ca-induced nuclear fusion–evaporation reactions, subsequently isolated in the recoil separators MARS at Texas A&M University, USA, and TASCA at GSI Darmstadt, Germany, before being thermalized in a buffer-gas-stopping cell. From the latter, the nuclear reaction products were extracted into gas-phase chromatographic systems, suitable for registering α-decaying short-lived radionuclides, such as isotopes of superheavy elements. Efficiencies of 21(3)% for <sup>204-209</sup>Fr were reached for the extraction into the optimized miniCOMPACT gas-chromatography setup, indicating that this technique enables the identification of isotopes of volatile as well as non-volatile elements. These studies guide the path towards chemical investigations of superheavy elements beyond flerovium, which are out of reach with currently used setups.</p>}}, author = {{Götz, S. and Raeder, S. and Block, M. and Düllmann, Ch E. and Folden, C. M. and Glennon, K. J. and Götz, M. and Hübner, A. and Jäger, E. and Kaleja, O. and Khuyagbaatar, J. and Kindler, B. and Krier, J. and Lens, L. and Lommel, B. and Mistry, A. K. and Mokry, Ch and Runke, J. and Såmark-Roth, A. and Tereshatov, E. E. and Thörle-Pospiech, P. and Volia, M. F. and Yakushev, A. and Yakusheva, V.}}, issn = {{0168-583X}}, keywords = {{Buffer gas cell; Extraction efficiency; Extraction time; Fusion–evaporation reactions; Gas catcher; Heavy elements; Superheavy elements}}, language = {{eng}}, month = {{11}}, pages = {{27--35}}, publisher = {{Elsevier}}, series = {{Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms}}, title = {{Rapid extraction of short-lived isotopes from a buffer gas cell for use in gas-phase chemistry experiments, Part II : On-line studies with short-lived accelerator-produced radionuclides}}, url = {{http://dx.doi.org/10.1016/j.nimb.2021.09.004}}, doi = {{10.1016/j.nimb.2021.09.004}}, volume = {{507}}, year = {{2021}}, }