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Sub-pixel correlation length neutron imaging : Spatially resolved scattering information of microstructures on a macroscopic scale

Harti, Ralph P. ; Strobl, Markus LU ; Betz, Benedikt ; Jefimovs, Konstantins ; Kagias, Matias LU and Grünzweig, Christian (2017) In Scientific Reports 7.
Abstract

Neutron imaging and scattering give data of significantly different nature and traditional methods leave a gap of accessible structure sizes at around 10 micrometers. Only in recent years overlap in the probed size ranges could be achieved by independent application of high resolution scattering and imaging methods, however without providing full structural information when microstructures vary on a macroscopic scale. In this study we show how quantitative neutron dark-field imaging with a novel experimental approach provides both sub-pixel resolution with respect to microscopic correlation lengths and imaging of macroscopic variations of the microstructure. Thus it provides combined information on multiple length scales. A dispersion... (More)

Neutron imaging and scattering give data of significantly different nature and traditional methods leave a gap of accessible structure sizes at around 10 micrometers. Only in recent years overlap in the probed size ranges could be achieved by independent application of high resolution scattering and imaging methods, however without providing full structural information when microstructures vary on a macroscopic scale. In this study we show how quantitative neutron dark-field imaging with a novel experimental approach provides both sub-pixel resolution with respect to microscopic correlation lengths and imaging of macroscopic variations of the microstructure. Thus it provides combined information on multiple length scales. A dispersion of micrometer sized polystyrene colloids was chosen as a model system to study gravity induced crystallisation of microspheres on a macro scale, including the identification of ordered as well as unordered phases. Our results pave the way to study heterogeneous systems locally in a previously impossible manner.

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author
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publishing date
type
Contribution to journal
publication status
published
subject
in
Scientific Reports
volume
7
article number
44588
publisher
Nature Publishing Group
external identifiers
  • pmid:28303923
  • scopus:85015310680
ISSN
2045-2322
DOI
10.1038/srep44588
language
English
LU publication?
no
additional info
Publisher Copyright: © The Author(s) 2017.
id
b2dc48ed-2c04-4bc0-9d69-e6b67321ae73
date added to LUP
2023-11-27 09:06:01
date last changed
2024-04-24 12:43:51
@article{b2dc48ed-2c04-4bc0-9d69-e6b67321ae73,
  abstract     = {{<p>Neutron imaging and scattering give data of significantly different nature and traditional methods leave a gap of accessible structure sizes at around 10 micrometers. Only in recent years overlap in the probed size ranges could be achieved by independent application of high resolution scattering and imaging methods, however without providing full structural information when microstructures vary on a macroscopic scale. In this study we show how quantitative neutron dark-field imaging with a novel experimental approach provides both sub-pixel resolution with respect to microscopic correlation lengths and imaging of macroscopic variations of the microstructure. Thus it provides combined information on multiple length scales. A dispersion of micrometer sized polystyrene colloids was chosen as a model system to study gravity induced crystallisation of microspheres on a macro scale, including the identification of ordered as well as unordered phases. Our results pave the way to study heterogeneous systems locally in a previously impossible manner.</p>}},
  author       = {{Harti, Ralph P. and Strobl, Markus and Betz, Benedikt and Jefimovs, Konstantins and Kagias, Matias and Grünzweig, Christian}},
  issn         = {{2045-2322}},
  language     = {{eng}},
  month        = {{03}},
  publisher    = {{Nature Publishing Group}},
  series       = {{Scientific Reports}},
  title        = {{Sub-pixel correlation length neutron imaging : Spatially resolved scattering information of microstructures on a macroscopic scale}},
  url          = {{http://dx.doi.org/10.1038/srep44588}},
  doi          = {{10.1038/srep44588}},
  volume       = {{7}},
  year         = {{2017}},
}