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Studies of phase-change materials using ultrafast X-ray diffraction

Nilsson, Eric LU (2025)
Abstract
This thesis is focused on the investigation of the ultrafast structural response of the phase change material (PCM) Ge$_2$Sb$_2$Te$_5$ following laser excitation. Phase change materials are a group of materials capable of rapid, non-volatile, switching between an amorphous and a crystalline phase. The two phases exhibit high optical and electrical contrast, meaning the optical reflectivity and the electrical conductivity differ significantly between the two phases. These properties make PCM suitable for data storage, and they have been widely used, mainly in DVD-RW discs. GST has been successfully used for Phase Change Random Access Memory (PCRAM), and the non-thermal excitation pathways have been the interest of numerous... (More)
This thesis is focused on the investigation of the ultrafast structural response of the phase change material (PCM) Ge$_2$Sb$_2$Te$_5$ following laser excitation. Phase change materials are a group of materials capable of rapid, non-volatile, switching between an amorphous and a crystalline phase. The two phases exhibit high optical and electrical contrast, meaning the optical reflectivity and the electrical conductivity differ significantly between the two phases. These properties make PCM suitable for data storage, and they have been widely used, mainly in DVD-RW discs. GST has been successfully used for Phase Change Random Access Memory (PCRAM), and the non-thermal excitation pathways have been the interest of numerous studies.

Conventionally, the phase change from the crystalline to the amorphous phase is driven by either optical or electric pulses on the order of 10 ns, where the material is melted and allowed to rapidly cool. If non-thermal pathways for amorphization exist, this could increase the write speed, up to 4 orders of magnitude.

This thesis presents ultrafast X-Ray Diffraction (XRD) studies investigating the ultrafast response of GST after femtosecond laser excitation, and compares the findings to previously suggested models, such as the suppression of the Peierls distortion, the umbrella flip model, and direct ultrafast amorphization. Furthermore, it is explained that the previous models do not satisfy the time-resolved behavior of the complete experimental findings, and a combination of these models is proposed as a more complete picture of the ultrafast dynamics. (Less)
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author
supervisor
opponent
  • Prof. Balling, Peter, Aarhus University, Denmark.
organization
publishing date
type
Thesis
publication status
published
subject
keywords
X-ray diffraction, TRXRD, Ge2Sb2Te5, GST, phase change material, PCM
pages
106 pages
publisher
Lund University , Department of physics
defense location
Lecture Hall Rydbergsalen, Department of Physics, Professorsgatan 1, Faculty of Engineering LTH, Lund University, Lund.
defense date
2025-11-28 13:15:00
ISBN
978-91-8104-748-6
978-91-8104-747-9
language
English
LU publication?
yes
id
b7f654f6-49c4-45eb-a560-c82d51a6d28b
date added to LUP
2025-11-03 11:53:24
date last changed
2025-11-05 13:08:29
@phdthesis{b7f654f6-49c4-45eb-a560-c82d51a6d28b,
  abstract     = {{This thesis is focused on the investigation of the ultrafast structural response of the phase change material (PCM) Ge$_2$Sb$_2$Te$_5$ following laser excitation. Phase change materials are a group of materials capable of rapid, non-volatile, switching between an amorphous and a crystalline phase. The two phases exhibit high optical and electrical contrast, meaning the optical reflectivity and the electrical conductivity differ significantly between the two phases. These properties make PCM suitable for data storage, and they have been widely used, mainly in DVD-RW discs. GST has been successfully used for Phase Change Random Access Memory (PCRAM), and the non-thermal excitation pathways have been the interest of numerous studies.<br/><br/>Conventionally, the phase change from the crystalline to the amorphous phase is driven by either optical or electric pulses on the order of 10 ns, where the material is melted and allowed to rapidly cool. If non-thermal pathways for amorphization exist, this could increase the write speed, up to 4 orders of magnitude.<br/><br/>This thesis presents ultrafast X-Ray Diffraction (XRD) studies investigating the ultrafast response of GST after femtosecond laser excitation, and compares the findings to previously suggested models, such as the suppression of the Peierls distortion, the umbrella flip model, and direct ultrafast amorphization. Furthermore, it is explained that the previous models do not satisfy the time-resolved behavior of the complete experimental findings, and a combination of these models is proposed as a more complete picture of the ultrafast dynamics.}},
  author       = {{Nilsson, Eric}},
  isbn         = {{978-91-8104-748-6}},
  keywords     = {{X-ray diffraction; TRXRD; Ge2Sb2Te5; GST; phase change material; PCM}},
  language     = {{eng}},
  publisher    = {{Lund University , Department of physics}},
  school       = {{Lund University}},
  title        = {{Studies of phase-change materials using ultrafast X-ray diffraction}},
  url          = {{https://lup.lub.lu.se/search/files/232052968/Eric_Nilsson_-_WEB.pdf}},
  year         = {{2025}},
}