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Magnesium/Nano-hydroxyapatite Composite for Bone Reconstruction : The Effect of Processing Method

Khodaei, Mohammad ; Nejatidanesh, Farahnaz ; Shirani, Mohammad Javad ; Iyengar, Srinivasan LU ; Sina, Hossein LU and Savabi, Omid (2020) In Journal of Bionic Engineering 17(1). p.92-99
Abstract

Nano-ceramic particles can serve as reinforcing agents for metallic materials to improve their mechanical properties. However, it is important to ensure chemical compatibility between the matrix and particles. In the present study, magnesium composites with and without nano-hydroxyapatite (nHA) particles were fabricated for bone reconstruction applications. Two different techniques were used, Conventional Sintering (CS) of powder compacts and Spark Plasma Sintering (SPS) of pre-compacted powder. Results showed that a 10 wt% addition of nHA particles to magnesium, followed by SPS improved the compression strength by 27%. CS did not lead to any significant improvement compared to SPS processing. X-ray diffraction data after CS revealed... (More)

Nano-ceramic particles can serve as reinforcing agents for metallic materials to improve their mechanical properties. However, it is important to ensure chemical compatibility between the matrix and particles. In the present study, magnesium composites with and without nano-hydroxyapatite (nHA) particles were fabricated for bone reconstruction applications. Two different techniques were used, Conventional Sintering (CS) of powder compacts and Spark Plasma Sintering (SPS) of pre-compacted powder. Results showed that a 10 wt% addition of nHA particles to magnesium, followed by SPS improved the compression strength by 27%. CS did not lead to any significant improvement compared to SPS processing. X-ray diffraction data after CS revealed the formation of unfavorable phases due to chemical reactions between nHA particles and the magnesium matrix, while these phases were absent after SPS processing. The mechanical properties of the specimens fabricated by CS were much inferior to those processed using SPS. The shorter processing time associated with SPS leaded to reduced interaction between nHA particles and the Mg-matrix, compared to CS.

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author
; ; ; ; and
organization
publishing date
type
Contribution to journal
publication status
published
subject
keywords
biomedical-materials, composite materials, in situ reaction, magnesium, nano-hydroxyapatite
in
Journal of Bionic Engineering
volume
17
issue
1
pages
8 pages
publisher
Science Press
external identifiers
  • scopus:85077888040
ISSN
1672-6529
DOI
10.1007/s42235-020-0007-6
language
English
LU publication?
yes
id
be542301-a6e9-4de3-89c5-bf9d0f8bef6e
date added to LUP
2021-01-04 10:53:37
date last changed
2022-04-26 22:58:05
@article{be542301-a6e9-4de3-89c5-bf9d0f8bef6e,
  abstract     = {{<p>Nano-ceramic particles can serve as reinforcing agents for metallic materials to improve their mechanical properties. However, it is important to ensure chemical compatibility between the matrix and particles. In the present study, magnesium composites with and without nano-hydroxyapatite (nHA) particles were fabricated for bone reconstruction applications. Two different techniques were used, Conventional Sintering (CS) of powder compacts and Spark Plasma Sintering (SPS) of pre-compacted powder. Results showed that a 10 wt% addition of nHA particles to magnesium, followed by SPS improved the compression strength by 27%. CS did not lead to any significant improvement compared to SPS processing. X-ray diffraction data after CS revealed the formation of unfavorable phases due to chemical reactions between nHA particles and the magnesium matrix, while these phases were absent after SPS processing. The mechanical properties of the specimens fabricated by CS were much inferior to those processed using SPS. The shorter processing time associated with SPS leaded to reduced interaction between nHA particles and the Mg-matrix, compared to CS.</p>}},
  author       = {{Khodaei, Mohammad and Nejatidanesh, Farahnaz and Shirani, Mohammad Javad and Iyengar, Srinivasan and Sina, Hossein and Savabi, Omid}},
  issn         = {{1672-6529}},
  keywords     = {{biomedical-materials; composite materials; in situ reaction; magnesium; nano-hydroxyapatite}},
  language     = {{eng}},
  number       = {{1}},
  pages        = {{92--99}},
  publisher    = {{Science Press}},
  series       = {{Journal of Bionic Engineering}},
  title        = {{Magnesium/Nano-hydroxyapatite Composite for Bone Reconstruction : The Effect of Processing Method}},
  url          = {{http://dx.doi.org/10.1007/s42235-020-0007-6}},
  doi          = {{10.1007/s42235-020-0007-6}},
  volume       = {{17}},
  year         = {{2020}},
}