Efficient Conversion of Biomass Derived Levulinic Acid to γ-Valerolactone Using Hydrosilylation
(2021) In European Journal of Organic Chemistry 2021(37). p.5243-5247- Abstract
Converting biomass into value-added chemicals is of significant interest and we report an efficient hydrosilylation to convert levulinic acid to γ-valerolactone using cost-effective silanes such as PMHS and TMDS with B(C6F5)3 as catalyst. This metal free methodology works at room temperature reaching TONs and TOFs up to 16000 and 2000 h−1. Insights into the reaction mechanism are reported.
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https://lup.lub.lu.se/record/c3dc10b4-9e79-4efd-be1d-75ac93d14bd7
- author
- Garg, Nitish K. LU ; Schmalz, Veronika ; Johnson, Magnus T. LU and Wendt, Ola F. LU
- organization
- publishing date
- 2021-10-07
- type
- Contribution to journal
- publication status
- published
- subject
- keywords
- Biomass, GVL, Hydrosilylation, Levulinic acid, Tris(pentafluorophenyl)borane
- in
- European Journal of Organic Chemistry
- volume
- 2021
- issue
- 37
- pages
- 5 pages
- publisher
- John Wiley & Sons Inc.
- external identifiers
-
- scopus:85117100146
- ISSN
- 1434-193X
- DOI
- 10.1002/ejoc.202100982
- language
- English
- LU publication?
- yes
- additional info
- Publisher Copyright: © 2021 The Authors. European Journal of Organic Chemistry published by Wiley-VCH GmbH
- id
- c3dc10b4-9e79-4efd-be1d-75ac93d14bd7
- date added to LUP
- 2021-10-26 13:15:40
- date last changed
- 2022-04-27 05:16:08
@article{c3dc10b4-9e79-4efd-be1d-75ac93d14bd7, abstract = {{<p>Converting biomass into value-added chemicals is of significant interest and we report an efficient hydrosilylation to convert levulinic acid to γ-valerolactone using cost-effective silanes such as PMHS and TMDS with B(C<sub>6</sub>F<sub>5</sub>)<sub>3</sub> as catalyst. This metal free methodology works at room temperature reaching TONs and TOFs up to 16000 and 2000 h<sup>−1</sup>. Insights into the reaction mechanism are reported.</p>}}, author = {{Garg, Nitish K. and Schmalz, Veronika and Johnson, Magnus T. and Wendt, Ola F.}}, issn = {{1434-193X}}, keywords = {{Biomass; GVL; Hydrosilylation; Levulinic acid; Tris(pentafluorophenyl)borane}}, language = {{eng}}, month = {{10}}, number = {{37}}, pages = {{5243--5247}}, publisher = {{John Wiley & Sons Inc.}}, series = {{European Journal of Organic Chemistry}}, title = {{Efficient Conversion of Biomass Derived Levulinic Acid to γ-Valerolactone Using Hydrosilylation}}, url = {{http://dx.doi.org/10.1002/ejoc.202100982}}, doi = {{10.1002/ejoc.202100982}}, volume = {{2021}}, year = {{2021}}, }