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Microwave-assisted solvent-free parallel synthesis of thioamides

Olsson, R. LU orcid ; Hansen, H. C. LU and Andersson, C. M. (2000) In Tetrahedron Letters 41(41). p.7947-7950
Abstract

Rapid parallel synthesis of thioamides is described. A library of amides, synthesised by mixing acyl chlorides and diamines, was transformed into the corresponding thioamides utilising Lawesson's reagent as the oxygen/sulphur exchange reagent. Purification by solid-phase extraction afforded the library members in adequate purities and yields. (C) 2000 Elsevier Science Ltd.

Please use this url to cite or link to this publication:
author
; and
publishing date
type
Contribution to journal
publication status
published
subject
keywords
Microwave, Parallel synthesis, Thioamide
in
Tetrahedron Letters
volume
41
issue
41
pages
7947 - 7950
publisher
Elsevier
external identifiers
  • scopus:0034619144
ISSN
0040-4039
DOI
10.1016/S0040-4039(00)01360-5
language
English
LU publication?
no
id
c87b2e1d-1cb9-4ba0-bcbd-2422f984c230
date added to LUP
2019-10-02 10:42:46
date last changed
2022-02-01 01:07:44
@article{c87b2e1d-1cb9-4ba0-bcbd-2422f984c230,
  abstract     = {{<p>Rapid parallel synthesis of thioamides is described. A library of amides, synthesised by mixing acyl chlorides and diamines, was transformed into the corresponding thioamides utilising Lawesson's reagent as the oxygen/sulphur exchange reagent. Purification by solid-phase extraction afforded the library members in adequate purities and yields. (C) 2000 Elsevier Science Ltd.</p>}},
  author       = {{Olsson, R. and Hansen, H. C. and Andersson, C. M.}},
  issn         = {{0040-4039}},
  keywords     = {{Microwave; Parallel synthesis; Thioamide}},
  language     = {{eng}},
  month        = {{10}},
  number       = {{41}},
  pages        = {{7947--7950}},
  publisher    = {{Elsevier}},
  series       = {{Tetrahedron Letters}},
  title        = {{Microwave-assisted solvent-free parallel synthesis of thioamides}},
  url          = {{http://dx.doi.org/10.1016/S0040-4039(00)01360-5}},
  doi          = {{10.1016/S0040-4039(00)01360-5}},
  volume       = {{41}},
  year         = {{2000}},
}