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Microwave-assisted solvent-free parallel synthesis of thioamides

Olsson, R. LU ; Hansen, H. C. LU and Andersson, C. M. (2000) In Tetrahedron Letters 41(41). p.7947-7950
Abstract

Rapid parallel synthesis of thioamides is described. A library of amides, synthesised by mixing acyl chlorides and diamines, was transformed into the corresponding thioamides utilising Lawesson's reagent as the oxygen/sulphur exchange reagent. Purification by solid-phase extraction afforded the library members in adequate purities and yields. (C) 2000 Elsevier Science Ltd.

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author
; and
publishing date
type
Contribution to journal
publication status
published
subject
keywords
Microwave, Parallel synthesis, Thioamide
in
Tetrahedron Letters
volume
41
issue
41
pages
7947 - 7950
publisher
Elsevier
external identifiers
  • scopus:0034619144
ISSN
0040-4039
DOI
10.1016/S0040-4039(00)01360-5
language
English
LU publication?
no
id
c87b2e1d-1cb9-4ba0-bcbd-2422f984c230
date added to LUP
2019-10-02 10:42:46
date last changed
2020-01-30 03:55:24
@article{c87b2e1d-1cb9-4ba0-bcbd-2422f984c230,
  abstract     = {<p>Rapid parallel synthesis of thioamides is described. A library of amides, synthesised by mixing acyl chlorides and diamines, was transformed into the corresponding thioamides utilising Lawesson's reagent as the oxygen/sulphur exchange reagent. Purification by solid-phase extraction afforded the library members in adequate purities and yields. (C) 2000 Elsevier Science Ltd.</p>},
  author       = {Olsson, R. and Hansen, H. C. and Andersson, C. M.},
  issn         = {0040-4039},
  language     = {eng},
  month        = {10},
  number       = {41},
  pages        = {7947--7950},
  publisher    = {Elsevier},
  series       = {Tetrahedron Letters},
  title        = {Microwave-assisted solvent-free parallel synthesis of thioamides},
  url          = {http://dx.doi.org/10.1016/S0040-4039(00)01360-5},
  doi          = {10.1016/S0040-4039(00)01360-5},
  volume       = {41},
  year         = {2000},
}