Fabrication and Characterization of a Thin-Layer Electrochemical Flow Cell and Its Application for Flow Analysis
(2011) In Analytical Letters 44(1-3). p.258-270- Abstract
- The design and fabrication of a home-made thin-layer electrochemical flow cell are reported. The performance and electrochemical characteristics of thin-layer cells are evaluated in terms of flow rate and channel thickness. The adaptability of the flow cell for amperometric and electrochemiluminescence measurements is demonstrated. Also, a flow injection method comprising electrochemical generation followed by spectrophotometric detection is proposed for determination of bromide using the fabricated cell. The influence of chemical, electrochemical, and flow parameters on the absorbance and current signals are investigated, and under optimized conditions, the analytical features of the proposed method with respect to bromide detection are... (More)
- The design and fabrication of a home-made thin-layer electrochemical flow cell are reported. The performance and electrochemical characteristics of thin-layer cells are evaluated in terms of flow rate and channel thickness. The adaptability of the flow cell for amperometric and electrochemiluminescence measurements is demonstrated. Also, a flow injection method comprising electrochemical generation followed by spectrophotometric detection is proposed for determination of bromide using the fabricated cell. The influence of chemical, electrochemical, and flow parameters on the absorbance and current signals are investigated, and under optimized conditions, the analytical features of the proposed method with respect to bromide detection are evaluated. (Less)
Please use this url to cite or link to this publication:
https://lup.lub.lu.se/record/1876656
- author
- Haghighi, Behzad ; Aghajari, Hamid ; Bozorgzadeh, Somayyeh and Gorton, Lo LU
- organization
- publishing date
- 2011
- type
- Contribution to journal
- publication status
- published
- subject
- keywords
- Amperometric detector, Bromide determination, Electrochemical flow, cell, Electrogenerated chemiluminescence detector, Thin-layer cell
- in
- Analytical Letters
- volume
- 44
- issue
- 1-3
- pages
- 258 - 270
- publisher
- Taylor & Francis
- external identifiers
-
- wos:000287494700020
- scopus:79951749184
- ISSN
- 0003-2719
- DOI
- 10.1080/00032719.2010.500763
- language
- English
- LU publication?
- yes
- additional info
- The information about affiliations in this record was updated in December 2015. The record was previously connected to the following departments: Analytical Chemistry (S/LTH) (011001004)
- id
- 4aa862ae-de23-408f-a02c-543b530e7f09 (old id 1876656)
- date added to LUP
- 2016-04-01 14:28:47
- date last changed
- 2022-01-28 00:51:48
@article{4aa862ae-de23-408f-a02c-543b530e7f09, abstract = {{The design and fabrication of a home-made thin-layer electrochemical flow cell are reported. The performance and electrochemical characteristics of thin-layer cells are evaluated in terms of flow rate and channel thickness. The adaptability of the flow cell for amperometric and electrochemiluminescence measurements is demonstrated. Also, a flow injection method comprising electrochemical generation followed by spectrophotometric detection is proposed for determination of bromide using the fabricated cell. The influence of chemical, electrochemical, and flow parameters on the absorbance and current signals are investigated, and under optimized conditions, the analytical features of the proposed method with respect to bromide detection are evaluated.}}, author = {{Haghighi, Behzad and Aghajari, Hamid and Bozorgzadeh, Somayyeh and Gorton, Lo}}, issn = {{0003-2719}}, keywords = {{Amperometric detector; Bromide determination; Electrochemical flow; cell; Electrogenerated chemiluminescence detector; Thin-layer cell}}, language = {{eng}}, number = {{1-3}}, pages = {{258--270}}, publisher = {{Taylor & Francis}}, series = {{Analytical Letters}}, title = {{Fabrication and Characterization of a Thin-Layer Electrochemical Flow Cell and Its Application for Flow Analysis}}, url = {{http://dx.doi.org/10.1080/00032719.2010.500763}}, doi = {{10.1080/00032719.2010.500763}}, volume = {{44}}, year = {{2011}}, }