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Multivariate optimization of supported liquid membrane extraction of biogenic amines from wine samples prior to liquid chromatography determination as dabsyl derivatives

Romero, R ; Jönsson, Jan Åke LU ; Gazquez, D ; Bagur, MG and Sanchez-Vinas, M (2002) In Journal of Separation Science 25(9). p.584-592
Abstract
The application of the supported liquid membrane (SLM) technique for the extraction of biogenic amines is presented. For the extraction of these compounds, the SLM system has been applied, using di-2-ethylhexyl phosphoric acid as an anionic carrier incorporated into the membrane phase. The optimization of the extraction process, involving the composition of membrane liquid, is discussed. The simultaneous optimization of the extraction efficiencies of all the amines is achieved by a desirability function, using experimental design strategies (Doehlert's and full factorial designs). The proposed method is evaluated for the extraction of biogenic amines from wines by comparing the extraction efficiency values with those obtained for a... (More)
The application of the supported liquid membrane (SLM) technique for the extraction of biogenic amines is presented. For the extraction of these compounds, the SLM system has been applied, using di-2-ethylhexyl phosphoric acid as an anionic carrier incorporated into the membrane phase. The optimization of the extraction process, involving the composition of membrane liquid, is discussed. The simultaneous optimization of the extraction efficiencies of all the amines is achieved by a desirability function, using experimental design strategies (Doehlert's and full factorial designs). The proposed method is evaluated for the extraction of biogenic amines from wines by comparing the extraction efficiency values with those obtained for a composite amine standard solution. The results show no significant differences. (Less)
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author
; ; ; and
organization
publishing date
type
Contribution to journal
publication status
published
subject
keywords
desirability function, multivariate optimization, biogenic amines, supported liquid membrane, wines
in
Journal of Separation Science
volume
25
issue
9
pages
584 - 592
publisher
John Wiley & Sons Inc.
external identifiers
  • wos:000176665600005
  • scopus:0036077951
ISSN
1615-9314
DOI
10.1002/1615-9314(20020601)25:9<584::AID-JSSC584>3.0.CO;2-F
language
English
LU publication?
yes
additional info
The information about affiliations in this record was updated in December 2015. The record was previously connected to the following departments: Analytical Chemistry (S/LTH) (011001004)
id
627436af-8731-401b-a81b-558f6caf2b31 (old id 334107)
date added to LUP
2016-04-01 12:12:19
date last changed
2022-01-27 00:21:54
@article{627436af-8731-401b-a81b-558f6caf2b31,
  abstract     = {{The application of the supported liquid membrane (SLM) technique for the extraction of biogenic amines is presented. For the extraction of these compounds, the SLM system has been applied, using di-2-ethylhexyl phosphoric acid as an anionic carrier incorporated into the membrane phase. The optimization of the extraction process, involving the composition of membrane liquid, is discussed. The simultaneous optimization of the extraction efficiencies of all the amines is achieved by a desirability function, using experimental design strategies (Doehlert's and full factorial designs). The proposed method is evaluated for the extraction of biogenic amines from wines by comparing the extraction efficiency values with those obtained for a composite amine standard solution. The results show no significant differences.}},
  author       = {{Romero, R and Jönsson, Jan Åke and Gazquez, D and Bagur, MG and Sanchez-Vinas, M}},
  issn         = {{1615-9314}},
  keywords     = {{desirability function; multivariate optimization; biogenic amines; supported liquid membrane; wines}},
  language     = {{eng}},
  number       = {{9}},
  pages        = {{584--592}},
  publisher    = {{John Wiley & Sons Inc.}},
  series       = {{Journal of Separation Science}},
  title        = {{Multivariate optimization of supported liquid membrane extraction of biogenic amines from wine samples prior to liquid chromatography determination as dabsyl derivatives}},
  url          = {{http://dx.doi.org/10.1002/1615-9314(20020601)25:9<584::AID-JSSC584>3.0.CO;2-F}},
  doi          = {{10.1002/1615-9314(20020601)25:9<584::AID-JSSC584>3.0.CO;2-F}},
  volume       = {{25}},
  year         = {{2002}},
}