Microwave-assisted solvent-free parallel synthesis of thioamides
(2000) In Tetrahedron Letters 41(41). p.7947-7950- Abstract
Rapid parallel synthesis of thioamides is described. A library of amides, synthesised by mixing acyl chlorides and diamines, was transformed into the corresponding thioamides utilising Lawesson's reagent as the oxygen/sulphur exchange reagent. Purification by solid-phase extraction afforded the library members in adequate purities and yields. (C) 2000 Elsevier Science Ltd.
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- author
- Olsson, R. LU ; Hansen, H. C. LU and Andersson, C. M.
- publishing date
- 2000-10-07
- type
- Contribution to journal
- publication status
- published
- subject
- keywords
- Microwave, Parallel synthesis, Thioamide
- in
- Tetrahedron Letters
- volume
- 41
- issue
- 41
- pages
- 7947 - 7950
- publisher
- Elsevier
- external identifiers
-
- scopus:0034619144
- ISSN
- 0040-4039
- DOI
- 10.1016/S0040-4039(00)01360-5
- language
- English
- LU publication?
- no
- id
- c87b2e1d-1cb9-4ba0-bcbd-2422f984c230
- date added to LUP
- 2019-10-02 10:42:46
- date last changed
- 2022-02-01 01:07:44
@article{c87b2e1d-1cb9-4ba0-bcbd-2422f984c230, abstract = {{<p>Rapid parallel synthesis of thioamides is described. A library of amides, synthesised by mixing acyl chlorides and diamines, was transformed into the corresponding thioamides utilising Lawesson's reagent as the oxygen/sulphur exchange reagent. Purification by solid-phase extraction afforded the library members in adequate purities and yields. (C) 2000 Elsevier Science Ltd.</p>}}, author = {{Olsson, R. and Hansen, H. C. and Andersson, C. M.}}, issn = {{0040-4039}}, keywords = {{Microwave; Parallel synthesis; Thioamide}}, language = {{eng}}, month = {{10}}, number = {{41}}, pages = {{7947--7950}}, publisher = {{Elsevier}}, series = {{Tetrahedron Letters}}, title = {{Microwave-assisted solvent-free parallel synthesis of thioamides}}, url = {{http://dx.doi.org/10.1016/S0040-4039(00)01360-5}}, doi = {{10.1016/S0040-4039(00)01360-5}}, volume = {{41}}, year = {{2000}}, }