Skip to main content

Lund University Publications

LUND UNIVERSITY LIBRARIES

The Mystery of the AuIn 1 : 1 Phase and Its Incommensurate Structural Variations

Folkers, Laura C. LU ; Simonov, Arkadiy ; Wang, Fei LU and Lidin, Sven LU (2018) In Inorganic Chemistry 57(5). p.2791-2796
Abstract

In this communication, the AuIn 1:1 phase (Naturwissenschaften, 1953, 40, 437, DOI: 10.1007/BF00590353), and its ordering behavior at various temperatures is investigated. To enable the growth of a X-ray suitable specimen, a tempering routine was established by the interpretation of a differential scanning calorimetry (DSC) study. In this way, good quality single crystals were grown and measured at the Crystal beamline at Synchrotron SOLEIL. From the acquired data, three variations of this structure could be found at temperatures of 400 °C and 300 °C and room temperature, with differing degrees of incommensurate modulation. Diffuse scattering found at 400 °C was interpreted with the help of a three-dimensional difference pair... (More)

In this communication, the AuIn 1:1 phase (Naturwissenschaften, 1953, 40, 437, DOI: 10.1007/BF00590353), and its ordering behavior at various temperatures is investigated. To enable the growth of a X-ray suitable specimen, a tempering routine was established by the interpretation of a differential scanning calorimetry (DSC) study. In this way, good quality single crystals were grown and measured at the Crystal beamline at Synchrotron SOLEIL. From the acquired data, three variations of this structure could be found at temperatures of 400 °C and 300 °C and room temperature, with differing degrees of incommensurate modulation. Diffuse scattering found at 400 °C was interpreted with the help of a three-dimensional difference pair distribution function (3D-ΔPDF) study.

(Less)
Please use this url to cite or link to this publication:
author
; ; and
organization
publishing date
type
Contribution to journal
publication status
published
subject
in
Inorganic Chemistry
volume
57
issue
5
pages
6 pages
publisher
The American Chemical Society (ACS)
external identifiers
  • pmid:29451387
  • scopus:85042903451
ISSN
0020-1669
DOI
10.1021/acs.inorgchem.7b03206
language
English
LU publication?
yes
id
083f9a07-9a67-4553-ab6b-9879623e9435
date added to LUP
2018-03-15 12:04:35
date last changed
2021-10-06 03:33:57
@article{083f9a07-9a67-4553-ab6b-9879623e9435,
  abstract     = {<p>In this communication, the AuIn 1:1 phase (Naturwissenschaften, 1953, 40, 437, DOI: 10.1007/BF00590353), and its ordering behavior at various temperatures is investigated. To enable the growth of a X-ray suitable specimen, a tempering routine was established by the interpretation of a differential scanning calorimetry (DSC) study. In this way, good quality single crystals were grown and measured at the Crystal beamline at Synchrotron SOLEIL. From the acquired data, three variations of this structure could be found at temperatures of 400 °C and 300 °C and room temperature, with differing degrees of incommensurate modulation. Diffuse scattering found at 400 °C was interpreted with the help of a three-dimensional difference pair distribution function (3D-ΔPDF) study.</p>},
  author       = {Folkers, Laura C. and Simonov, Arkadiy and Wang, Fei and Lidin, Sven},
  issn         = {0020-1669},
  language     = {eng},
  month        = {03},
  number       = {5},
  pages        = {2791--2796},
  publisher    = {The American Chemical Society (ACS)},
  series       = {Inorganic Chemistry},
  title        = {The Mystery of the AuIn 1 : 1 Phase and Its Incommensurate Structural Variations},
  url          = {http://dx.doi.org/10.1021/acs.inorgchem.7b03206},
  doi          = {10.1021/acs.inorgchem.7b03206},
  volume       = {57},
  year         = {2018},
}