Mild Microwave-Assisted Hydrolysis of Acetals Under Solvent-Free Conditions
(2004) In Synthetic Communications 34(22). p.4153-4158- Abstract
- Acetals are efficiently hydrolyzed with silica gel‐supported pyridinium tosylate moistened with water in solvent‐free conditions under microwave irradiation. The method is efficient and mild, with acid‐sensitive 3‐hydroxyacetals and 3‐methoxyacetals being hydrolyzed in minutes in good yields.
Please use this url to cite or link to this publication:
https://lup.lub.lu.se/record/141500
- author
- He, Yanhong LU ; Johansson, Martin H LU and Sterner, Olov LU
- organization
- publishing date
- 2004
- type
- Contribution to journal
- publication status
- published
- subject
- in
- Synthetic Communications
- volume
- 34
- issue
- 22
- pages
- 4153 - 4158
- publisher
- Marcel Dekker
- external identifiers
-
- wos:000225241500013
- scopus:8644289269
- ISSN
- 0039-7911
- DOI
- 10.1081/SCC-200036616
- language
- English
- LU publication?
- yes
- additional info
- The information about affiliations in this record was updated in December 2015. The record was previously connected to the following departments: Organic chemistry (S/LTH) (011001240)
- id
- b5dd0799-4fde-491f-b445-2be8941f188d (old id 141500)
- date added to LUP
- 2016-04-01 16:36:07
- date last changed
- 2022-01-28 20:50:26
@article{b5dd0799-4fde-491f-b445-2be8941f188d, abstract = {{Acetals are efficiently hydrolyzed with silica gel‐supported pyridinium tosylate moistened with water in solvent‐free conditions under microwave irradiation. The method is efficient and mild, with acid‐sensitive 3‐hydroxyacetals and 3‐methoxyacetals being hydrolyzed in minutes in good yields.}}, author = {{He, Yanhong and Johansson, Martin H and Sterner, Olov}}, issn = {{0039-7911}}, language = {{eng}}, number = {{22}}, pages = {{4153--4158}}, publisher = {{Marcel Dekker}}, series = {{Synthetic Communications}}, title = {{Mild Microwave-Assisted Hydrolysis of Acetals Under Solvent-Free Conditions}}, url = {{http://dx.doi.org/10.1081/SCC-200036616}}, doi = {{10.1081/SCC-200036616}}, volume = {{34}}, year = {{2004}}, }