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Mild Microwave-Assisted Hydrolysis of Acetals Under Solvent-Free Conditions

He, Yanhong LU ; Johansson, Martin H LU and Sterner, Olov LU (2004) In Synthetic Communications 34(22). p.4153-4158
Abstract
Acetals are efficiently hydrolyzed with silica gel‐supported pyridinium tosylate moistened with water in solvent‐free conditions under microwave irradiation. The method is efficient and mild, with acid‐sensitive 3‐hydroxyacetals and 3‐methoxyacetals being hydrolyzed in minutes in good yields.
Please use this url to cite or link to this publication:
author
organization
publishing date
type
Contribution to journal
publication status
published
subject
in
Synthetic Communications
volume
34
issue
22
pages
4153 - 4158
publisher
Marcel Dekker
external identifiers
  • wos:000225241500013
  • scopus:8644289269
ISSN
0039-7911
DOI
10.1081/SCC-200036616
language
English
LU publication?
yes
id
b5dd0799-4fde-491f-b445-2be8941f188d (old id 141500)
date added to LUP
2007-07-10 10:50:31
date last changed
2017-02-19 04:14:18
@article{b5dd0799-4fde-491f-b445-2be8941f188d,
  abstract     = {Acetals are efficiently hydrolyzed with silica gel‐supported pyridinium tosylate moistened with water in solvent‐free conditions under microwave irradiation. The method is efficient and mild, with acid‐sensitive 3‐hydroxyacetals and 3‐methoxyacetals being hydrolyzed in minutes in good yields.},
  author       = {He, Yanhong and Johansson, Martin H and Sterner, Olov},
  issn         = {0039-7911},
  language     = {eng},
  number       = {22},
  pages        = {4153--4158},
  publisher    = {Marcel Dekker},
  series       = {Synthetic Communications},
  title        = {Mild Microwave-Assisted Hydrolysis of Acetals Under Solvent-Free Conditions},
  url          = {http://dx.doi.org/10.1081/SCC-200036616},
  volume       = {34},
  year         = {2004},
}