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Selective and simultaneous determination of trace bisphenol A and tebuconazole in vegetable and juice samples by membrane-based molecularly imprinted solid-phase extraction and HPLC

Wu, Ya-ting ; Zhang, Yan-hong ; Zhang, Meng ; Liu, Fei ; Wan, Ying-chun ; Huang, Zheng ; Ye, Lei LU orcid ; Zhou, Qi ; Shi, Yun and Lu, Bin (2014) In Food Chemistry 164. p.527-535
Abstract
Nanofibrous molecularly imprinted membranes (nano-MIMs) with multi-analyte selectivity were prepared by encapsulating two types of molecularly imprinted polymer nanoparticles (MIP-NPs) into electrospun polyvinyl alcohol nanofibers. The obtained nano-MIMs maintained high molecular selectivity offered by each of the MIP-NPs. Nano-MIM embedding BPA-imprinted nanoparticles and TBZ-imprinted nanoparticles together showed the highest binding selectivity for acid bisphenol A (BPA) and basic tebuconazole (TBZ). This nano-MIM was used as affinity material of membrane-based molecularly imprinted solid-phase extraction (m-MISPE) to extract trace BPA and TBZ in vegetables and juices simultaneously. The recoveries of BPA and TBZ from different samples... (More)
Nanofibrous molecularly imprinted membranes (nano-MIMs) with multi-analyte selectivity were prepared by encapsulating two types of molecularly imprinted polymer nanoparticles (MIP-NPs) into electrospun polyvinyl alcohol nanofibers. The obtained nano-MIMs maintained high molecular selectivity offered by each of the MIP-NPs. Nano-MIM embedding BPA-imprinted nanoparticles and TBZ-imprinted nanoparticles together showed the highest binding selectivity for acid bisphenol A (BPA) and basic tebuconazole (TBZ). This nano-MIM was used as affinity material of membrane-based molecularly imprinted solid-phase extraction (m-MISPE) to extract trace BPA and TBZ in vegetables and juices simultaneously. The recoveries of BPA and TBZ from different samples were higher than 70.33% with RSDs lower than 9.57%. m-MISPE gave better HPLC separation efficiencies and higher recoveries than conventional SPE based on C18/SCX. Multi-analyte selective m-MISPE combined with HPLC realized selective and simultaneous determination of several trace analytes with opposite charges/polarities in different food samples. (C) 2014 Elsevier Ltd. All rights reserved. (Less)
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author
; ; ; ; ; ; ; ; and
organization
publishing date
type
Contribution to journal
publication status
published
subject
keywords
Molecularly imprinted polymers, Electrospun nanofibrous membrane, Bisphenol A, Tebuconazole, Membrane-based molecularly imprinted, solid-phase extraction, Vegetable and juice samples
in
Food Chemistry
volume
164
pages
527 - 535
publisher
Elsevier
external identifiers
  • pmid:24996366
  • wos:000339457500071
  • scopus:84902185376
  • pmid:24996366
ISSN
1873-7072
DOI
10.1016/j.foodchem.2014.05.071
language
English
LU publication?
yes
id
a038ecb6-ccf0-4312-97e8-cf459983ee5f (old id 4590545)
date added to LUP
2016-04-01 14:08:53
date last changed
2021-10-06 04:24:49
@article{a038ecb6-ccf0-4312-97e8-cf459983ee5f,
  abstract     = {Nanofibrous molecularly imprinted membranes (nano-MIMs) with multi-analyte selectivity were prepared by encapsulating two types of molecularly imprinted polymer nanoparticles (MIP-NPs) into electrospun polyvinyl alcohol nanofibers. The obtained nano-MIMs maintained high molecular selectivity offered by each of the MIP-NPs. Nano-MIM embedding BPA-imprinted nanoparticles and TBZ-imprinted nanoparticles together showed the highest binding selectivity for acid bisphenol A (BPA) and basic tebuconazole (TBZ). This nano-MIM was used as affinity material of membrane-based molecularly imprinted solid-phase extraction (m-MISPE) to extract trace BPA and TBZ in vegetables and juices simultaneously. The recoveries of BPA and TBZ from different samples were higher than 70.33% with RSDs lower than 9.57%. m-MISPE gave better HPLC separation efficiencies and higher recoveries than conventional SPE based on C18/SCX. Multi-analyte selective m-MISPE combined with HPLC realized selective and simultaneous determination of several trace analytes with opposite charges/polarities in different food samples. (C) 2014 Elsevier Ltd. All rights reserved.},
  author       = {Wu, Ya-ting and Zhang, Yan-hong and Zhang, Meng and Liu, Fei and Wan, Ying-chun and Huang, Zheng and Ye, Lei and Zhou, Qi and Shi, Yun and Lu, Bin},
  issn         = {1873-7072},
  language     = {eng},
  pages        = {527--535},
  publisher    = {Elsevier},
  series       = {Food Chemistry},
  title        = {Selective and simultaneous determination of trace bisphenol A and tebuconazole in vegetable and juice samples by membrane-based molecularly imprinted solid-phase extraction and HPLC},
  url          = {http://dx.doi.org/10.1016/j.foodchem.2014.05.071},
  doi          = {10.1016/j.foodchem.2014.05.071},
  volume       = {164},
  year         = {2014},
}