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Ex‐situ synchrotron X‐ray diffraction study of CO2 corrosion‐induced surface scales developed in low‐alloy steel with different initial microstructure

Haratian, Saber ; Gupta, Kapil Kumar ; Larsson, Alfred LU ; Abbondanza, Giuseppe LU ; Bartawi, Emad Hasan ; Carlà, Francesco ; Lundgren, Edvin LU and Ambat, Rajan (2023) In Corrosion Science 222.
Abstract

The CO2 corrosion-induced scale developed in the surface region of the low-grade carbon steel is thoroughly investigated to understand the corrosion mechanisms involved during exposure to CO2-saturated aqueous environments. In this work, in addition to the electron microscopy and lab-source X-ray diffraction (XRD) methods, ex-situ depth-resolved phase identification of the corrosion scales developed on steel with different initial microstructures is performed using synchrotron grazing incidence XRD at different incidence angles. The CO2 corrosion mechanism is discussed considering the observed distribution of the corrosion products formed at a different depth relative to the time of electrochemical... (More)

The CO2 corrosion-induced scale developed in the surface region of the low-grade carbon steel is thoroughly investigated to understand the corrosion mechanisms involved during exposure to CO2-saturated aqueous environments. In this work, in addition to the electron microscopy and lab-source X-ray diffraction (XRD) methods, ex-situ depth-resolved phase identification of the corrosion scales developed on steel with different initial microstructures is performed using synchrotron grazing incidence XRD at different incidence angles. The CO2 corrosion mechanism is discussed considering the observed distribution of the corrosion products formed at a different depth relative to the time of electrochemical exposure of the steels.

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author
; ; ; ; ; ; and
organization
publishing date
type
Contribution to journal
publication status
published
subject
keywords
CO corrosion, Depth-resolved phase identification, Grazing incidence X-ray diffraction, Scaling
in
Corrosion Science
volume
222
article number
111387
publisher
Elsevier
external identifiers
  • scopus:85165366965
ISSN
0010-938X
DOI
10.1016/j.corsci.2023.111387
language
English
LU publication?
yes
id
4e8ed7bc-c56b-47b0-8dca-72a621287359
date added to LUP
2023-09-04 11:08:17
date last changed
2023-11-08 10:39:39
@article{4e8ed7bc-c56b-47b0-8dca-72a621287359,
  abstract     = {{<p>The CO<sub>2</sub> corrosion-induced scale developed in the surface region of the low-grade carbon steel is thoroughly investigated to understand the corrosion mechanisms involved during exposure to CO<sub>2</sub>-saturated aqueous environments. In this work, in addition to the electron microscopy and lab-source X-ray diffraction (XRD) methods, ex-situ depth-resolved phase identification of the corrosion scales developed on steel with different initial microstructures is performed using synchrotron grazing incidence XRD at different incidence angles. The CO<sub>2</sub> corrosion mechanism is discussed considering the observed distribution of the corrosion products formed at a different depth relative to the time of electrochemical exposure of the steels.</p>}},
  author       = {{Haratian, Saber and Gupta, Kapil Kumar and Larsson, Alfred and Abbondanza, Giuseppe and Bartawi, Emad Hasan and Carlà, Francesco and Lundgren, Edvin and Ambat, Rajan}},
  issn         = {{0010-938X}},
  keywords     = {{CO corrosion; Depth-resolved phase identification; Grazing incidence X-ray diffraction; Scaling}},
  language     = {{eng}},
  publisher    = {{Elsevier}},
  series       = {{Corrosion Science}},
  title        = {{Ex‐situ synchrotron X‐ray diffraction study of CO<sub>2</sub> corrosion‐induced surface scales developed in low‐alloy steel with different initial microstructure}},
  url          = {{http://dx.doi.org/10.1016/j.corsci.2023.111387}},
  doi          = {{10.1016/j.corsci.2023.111387}},
  volume       = {{222}},
  year         = {{2023}},
}