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Photocatalytic setup for in situ and operando ambient-pressure X-ray photoelectron spectroscopy at MAX IV Laboratory

Klyushin, Alexander LU ; Ghosalya, Manoj ; Kokkonen, Esko LU orcid ; Eads, Calley LU orcid ; Jones, Rosemary LU ; Nalajala, Naresh ; Gopinath, Chinnakonda S. and Urpelainen, Samuli LU (2023) In Journal of Synchrotron Radiation 30(3). p.613-619
Abstract

The Ambient-Pressure X-ray Photoelectron Spectroscopy (APXPS) endstation at the SPECIES beamline at MAX IV Laboratory has been improved. The latest upgrades help in performing photo-assisted experiments under operando conditions in the mbar pressure range using gas and vapour mixtures whilst also reducing beam damage to the sample caused by X-ray irradiation. This article reports on endstation upgrades for APXPS and examples of scientific cases of in situ photocatalysis, photoreduction and photo-assisted atomic layer deposition (photo-ALD).

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author
; ; ; ; ; ; and
organization
publishing date
type
Contribution to journal
publication status
published
subject
keywords
APXPS, photo-ALD, photocatalysis, solar simulator
in
Journal of Synchrotron Radiation
volume
30
issue
3
pages
7 pages
publisher
International Union of Crystallography
external identifiers
  • pmid:37067260
  • scopus:85159550333
ISSN
0909-0495
DOI
10.1107/S1600577523002801
language
English
LU publication?
yes
additional info
Publisher Copyright: © 2023 International Union of Crystallography. All rights reserved.
id
55784ad7-8569-4c66-a0fe-4d2b4045363b
date added to LUP
2023-06-05 08:11:50
date last changed
2025-10-20 10:03:52
@article{55784ad7-8569-4c66-a0fe-4d2b4045363b,
  abstract     = {{<p>The Ambient-Pressure X-ray Photoelectron Spectroscopy (APXPS) endstation at the SPECIES beamline at MAX IV Laboratory has been improved. The latest upgrades help in performing photo-assisted experiments under operando conditions in the mbar pressure range using gas and vapour mixtures whilst also reducing beam damage to the sample caused by X-ray irradiation. This article reports on endstation upgrades for APXPS and examples of scientific cases of in situ photocatalysis, photoreduction and photo-assisted atomic layer deposition (photo-ALD).</p>}},
  author       = {{Klyushin, Alexander and Ghosalya, Manoj and Kokkonen, Esko and Eads, Calley and Jones, Rosemary and Nalajala, Naresh and Gopinath, Chinnakonda S. and Urpelainen, Samuli}},
  issn         = {{0909-0495}},
  keywords     = {{APXPS; photo-ALD; photocatalysis; solar simulator}},
  language     = {{eng}},
  month        = {{04}},
  number       = {{3}},
  pages        = {{613--619}},
  publisher    = {{International Union of Crystallography}},
  series       = {{Journal of Synchrotron Radiation}},
  title        = {{Photocatalytic setup for in situ and operando ambient-pressure X-ray photoelectron spectroscopy at MAX IV Laboratory}},
  url          = {{http://dx.doi.org/10.1107/S1600577523002801}},
  doi          = {{10.1107/S1600577523002801}},
  volume       = {{30}},
  year         = {{2023}},
}