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Selective pressurized hot water extraction of nutritious macro-nutrients vs. micro-nutrients in Moringa oleifera leaves—a chemometric approach

Nuapia, Yannick LU ; Al-Hamimi, Said ; Matshediso, Phatsimo G. ; Cukrowska, Ewa ; Tutu, Hlanganani ; Turner, Charlotta LU orcid and Chimuka, Luke LU (2020) In Analytical and Bioanalytical Chemistry 412(11). p.2495-2503
Abstract

Moringa oleifera leaves are widely used in traditional medicine as a food supplement because they are high in essential and nutritious content. Pressurized hot water extraction (PHWE), which is a green approach, was used for the recovery of the macro-nutrient and micro-nutrient elements from dried leaf powder of Moringa oleifera. In this study, response surface methodology was applied to assess the influence of temperature (50–200 °C) and time (5–60 min) on the extractability pattern of macro-nutrient and micro-nutrient elements from the leaves of Moringa oleifera when processed by PHWE. The quantification of macro-nutrient elements such as Ca, K and Mg and micro-nutrient elements like Al, Co, Cr, Cu, Fe, Ni and Zn from the leaves was... (More)

Moringa oleifera leaves are widely used in traditional medicine as a food supplement because they are high in essential and nutritious content. Pressurized hot water extraction (PHWE), which is a green approach, was used for the recovery of the macro-nutrient and micro-nutrient elements from dried leaf powder of Moringa oleifera. In this study, response surface methodology was applied to assess the influence of temperature (50–200 °C) and time (5–60 min) on the extractability pattern of macro-nutrient and micro-nutrient elements from the leaves of Moringa oleifera when processed by PHWE. The quantification of macro-nutrient elements such as Ca, K and Mg and micro-nutrient elements like Al, Co, Cr, Cu, Fe, Ni and Zn from the leaves was determined using inductively coupled plasma optical emission spectroscopy (ICP-OES). Obtained results revealed that the extraction of macro-nutrient elements from the Moringa oleifera leaves was enhanced by increasing the extraction time more than the extraction temperature. On the contrary, the amounts of extractable micro-nutrient elements were increased by increasing the extraction temperature. Hence, the recovery for macro-nutrient elements ranged from 88 to 98% while for micro-nutrients it ranged from 21 to 46%. This implies that macro-nutrient elements are extracted with relatively high selectivity in relation to micro-nutrient elements in Moringa dried leaf powder using the PHWE technique.

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author
; ; ; ; ; and
organization
publishing date
type
Contribution to journal
publication status
published
subject
keywords
Macro-nutrient and micro-nutrient elements, Moringa oleifera, Pressurized hot water extraction, Response surface
in
Analytical and Bioanalytical Chemistry
volume
412
issue
11
pages
9 pages
publisher
Springer
external identifiers
  • scopus:85078959881
  • pmid:32034455
ISSN
1618-2642
DOI
10.1007/s00216-020-02472-4
language
English
LU publication?
yes
id
69aed3c8-faf0-4b96-bb21-2a27eaf77c0b
date added to LUP
2020-02-17 14:33:47
date last changed
2024-11-28 03:50:38
@article{69aed3c8-faf0-4b96-bb21-2a27eaf77c0b,
  abstract     = {{<p>Moringa oleifera leaves are widely used in traditional medicine as a food supplement because they are high in essential and nutritious content. Pressurized hot water extraction (PHWE), which is a green approach, was used for the recovery of the macro-nutrient and micro-nutrient elements from dried leaf powder of Moringa oleifera. In this study, response surface methodology was applied to assess the influence of temperature (50–200 °C) and time (5–60 min) on the extractability pattern of macro-nutrient and micro-nutrient elements from the leaves of Moringa oleifera when processed by PHWE. The quantification of macro-nutrient elements such as Ca, K and Mg and micro-nutrient elements like Al, Co, Cr, Cu, Fe, Ni and Zn from the leaves was determined using inductively coupled plasma optical emission spectroscopy (ICP-OES). Obtained results revealed that the extraction of macro-nutrient elements from the Moringa oleifera leaves was enhanced by increasing the extraction time more than the extraction temperature. On the contrary, the amounts of extractable micro-nutrient elements were increased by increasing the extraction temperature. Hence, the recovery for macro-nutrient elements ranged from 88 to 98% while for micro-nutrients it ranged from 21 to 46%. This implies that macro-nutrient elements are extracted with relatively high selectivity in relation to micro-nutrient elements in Moringa dried leaf powder using the PHWE technique.</p>}},
  author       = {{Nuapia, Yannick and Al-Hamimi, Said and Matshediso, Phatsimo G. and Cukrowska, Ewa and Tutu, Hlanganani and Turner, Charlotta and Chimuka, Luke}},
  issn         = {{1618-2642}},
  keywords     = {{Macro-nutrient and micro-nutrient elements; Moringa oleifera; Pressurized hot water extraction; Response surface}},
  language     = {{eng}},
  number       = {{11}},
  pages        = {{2495--2503}},
  publisher    = {{Springer}},
  series       = {{Analytical and Bioanalytical Chemistry}},
  title        = {{Selective pressurized hot water extraction of nutritious macro-nutrients vs. micro-nutrients in Moringa oleifera leaves—a chemometric approach}},
  url          = {{http://dx.doi.org/10.1007/s00216-020-02472-4}},
  doi          = {{10.1007/s00216-020-02472-4}},
  volume       = {{412}},
  year         = {{2020}},
}