Three-dimensional diffraction mapping by tuning the X-ray energy
(2011) In Journal of Synchrotron Radiation 18(3). p.413-417- Abstract
Three-dimensional reciprocal-space maps of a single SiGe island around the Si(004) Bragg peak are recorded using an energy-tuning technique with a microfocused X-ray beam with compound refractive lenses as focusing optics. The map is in agreement with simulated data as well as with a map recorded by an ordinary rocking-curve scan. The energy-tuning approach circumvents both the comparatively large sphere of confusion of diffractometers compared with nanostructures and vibrations induced by motors. Thus, this method offers new possibilities for novel combinations of three-dimensional micro- and nano-focused X-ray diffraction with complex in situ sample environments such as scanning probe microscopes.
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https://lup.lub.lu.se/record/bdd531cd-5993-40b5-8b91-01e7eb5e5454
- author
- Cornelius, T. W. ; Carbone, D. LU ; Jacques, V. L.R. ; Schülli, T. U. and Metzger, T. H.
- publishing date
- 2011-05
- type
- Contribution to journal
- publication status
- published
- keywords
- energy scan, nanofocused and microfocused XRD, three-dimensional reciprocal-space mapping, X-ray diffraction
- in
- Journal of Synchrotron Radiation
- volume
- 18
- issue
- 3
- pages
- 5 pages
- publisher
- International Union of Crystallography
- external identifiers
-
- scopus:79955562523
- ISSN
- 0909-0495
- DOI
- 10.1107/S0909049511003190
- language
- English
- LU publication?
- no
- id
- bdd531cd-5993-40b5-8b91-01e7eb5e5454
- date added to LUP
- 2021-12-15 11:49:13
- date last changed
- 2022-03-19 05:34:11
@article{bdd531cd-5993-40b5-8b91-01e7eb5e5454, abstract = {{<p>Three-dimensional reciprocal-space maps of a single SiGe island around the Si(004) Bragg peak are recorded using an energy-tuning technique with a microfocused X-ray beam with compound refractive lenses as focusing optics. The map is in agreement with simulated data as well as with a map recorded by an ordinary rocking-curve scan. The energy-tuning approach circumvents both the comparatively large sphere of confusion of diffractometers compared with nanostructures and vibrations induced by motors. Thus, this method offers new possibilities for novel combinations of three-dimensional micro- and nano-focused X-ray diffraction with complex in situ sample environments such as scanning probe microscopes.</p>}}, author = {{Cornelius, T. W. and Carbone, D. and Jacques, V. L.R. and Schülli, T. U. and Metzger, T. H.}}, issn = {{0909-0495}}, keywords = {{energy scan; nanofocused and microfocused XRD; three-dimensional reciprocal-space mapping; X-ray diffraction}}, language = {{eng}}, number = {{3}}, pages = {{413--417}}, publisher = {{International Union of Crystallography}}, series = {{Journal of Synchrotron Radiation}}, title = {{Three-dimensional diffraction mapping by tuning the X-ray energy}}, url = {{http://dx.doi.org/10.1107/S0909049511003190}}, doi = {{10.1107/S0909049511003190}}, volume = {{18}}, year = {{2011}}, }